5-amino-1,3-dibenzyl-6-phenethyl pyrimidine-2,4(1H,3H)-dione

Base Information

Chemical Name:5-amino-1,3-dibenzyl-6-phenethyl pyrimidine-2,4(1H,3H)-dione
CAS No.:950664-86-5
Molecular Formula:C₂₆H₂₅N₃O₂
Molecular Weight:411.503
Hs Code.:

Synonyms:5-amino-1,3-dibenzyl-6-phenethyl pyrimidine-2,4(1H,3H)-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-amino-1,3-dibenzyl-6-phenethyl pyrimidine-2,4(1H,3H)-dione

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Technology Process of 5-amino-1,3-dibenzyl-6-phenethyl pyrimidine-2,4(1H,3H)-dione

There total 2 articles about 5-amino-1,3-dibenzyl-6-phenethyl pyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 950664-85-4
1,3-dibenzyl-5-nitro-6-phenethylpyrimidine-2,4(1H,3H)-dione

: 950664-86-5
5-amino-1,3-dibenzyl-6-phenethyl pyrimidine-2,4(1H,3H)-dione

Guidance literature:: With sodium dithionite; In methanol; for 0.5h; Heating;
DOI:10.1080/00397910701412737

Reference yield:

: 626-48-2
6-Methyluracil

: 950664-86-5
5-amino-1,3-dibenzyl-6-phenethyl pyrimidine-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / P₂O₅; fuming HNO₃ / cooling

2: 66 percent / NaH / dimethylformamide / 3 h / 20 °C

3: 89 percent / Na₂S₂O₄ / methanol / 0.5 h / Heating

With sodium dithionite; nitric acid; phosphorus pentoxide; sodium hydride; In methanol; N,N-dimethyl-formamide;
DOI:10.1080/00397910701412737