Technology Process of C16H20N6O2
There total 4 articles about C16H20N6O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 95 percent / NaN3 / dimethylsulfoxide / 3 h / 80 °C
2.1: NaNO2; H2SO4 / acetic acid; H2O / 0.08 h / 0 °C
2.2: 75 percent / dimethylformamide; acetic acid; H2O / 12 h / 0 °C
3.1: 211 mg / triphenylphosphane / tetrahydrofuran; H2O / 18 h / 20 - 50 °C
With
sodium azide; sulfuric acid; triphenylphosphine; sodium nitrite;
In
tetrahydrofuran; water; acetic acid; dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2006.11.066
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: NaNO2; H2SO4 / acetic acid; H2O / 0.08 h / 0 °C
1.2: 75 percent / dimethylformamide; acetic acid; H2O / 12 h / 0 °C
2.1: 211 mg / triphenylphosphane / tetrahydrofuran; H2O / 18 h / 20 - 50 °C
With
sulfuric acid; triphenylphosphine; sodium nitrite;
In
tetrahydrofuran; water; acetic acid;
DOI:10.1016/j.tetlet.2006.11.066