6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

Base Information

Chemical Name:6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester
CAS No.:179486-15-8
Molecular Formula:C₃₈H₅₀N₂O₉
Molecular Weight:678.823
Hs Code.:

6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

Synonyms:6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

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Chemical Property of 6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

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Technology Process of 6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

There total 4 articles about 6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54664-43-6
4'-benzo-15-crown-5-carboxylic acid chloride

: 179486-14-7
4-[4-(11-Hydroxy-undecyloxy)-phenylazo]-phenol

: 179486-15-8
6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

Guidance literature:: With pyridine; In tetrahydrofuran; at 40 ℃; Yield given;
DOI:10.1246/bcsj.69.2123

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 179486-15-8
6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 31 percent / KOH

2: 29.8 percent / KOH, NaI / ethanol / 24 h / Heating

3: Py / tetrahydrofuran / 40 °C

With pyridine; potassium hydroxide; sodium iodide; In tetrahydrofuran; ethanol;
DOI:10.1246/bcsj.69.2123

Reference yield:

: 56683-55-7
2,3-(4'-carboxybenzo)-1,4,7,10,13-pentaoxacyclopentadeca-2-ene

: 179486-15-8
6,7,9,10,12,13,15,16-Octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecene-2-carboxylic acid 11-[4-(4-hydroxy-phenylazo)-phenoxy]-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / CHCl₃ / 3 h / Heating

2: Py / tetrahydrofuran / 40 °C

With pyridine; thionyl chloride; In tetrahydrofuran; chloroform;
DOI:10.1246/bcsj.69.2123