(S)-2-[(R)-azido(phenyl)methyl]-1-benzylpyrrolidine

Base Information

Chemical Name:(S)-2-[(R)-azido(phenyl)methyl]-1-benzylpyrrolidine
CAS No.:1448991-14-7
Molecular Formula:C₁₈H₂₀N₄
Molecular Weight:292.384
Hs Code.:

Synonyms:(S)-2-[(R)-azido(phenyl)methyl]-1-benzylpyrrolidine

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Chemical Property of (S)-2-[(R)-azido(phenyl)methyl]-1-benzylpyrrolidine

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Technology Process of (S)-2-[(R)-azido(phenyl)methyl]-1-benzylpyrrolidine

There total 12 articles about (S)-2-[(R)-azido(phenyl)methyl]-1-benzylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (S)-tert-butyl 2-((R)-azido(phenyl)methyl)pyrrolidine-1-carboxylate

: 100-39-0
benzyl bromide

: 1448991-14-7
(S)-2-[(R)-azido(phenyl)methyl]-1-benzylpyrrolidine

Guidance literature:: (S)-tert-butyl 2-((R)-azido(phenyl)methyl)pyrrolidine-1-carboxylate; With trifluoroacetic acid; In dichloromethane;

benzyl bromide; With potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 10h;

Reference yield: 89.0%

: (2S,3R)-1-benzyl-3-chloro-2-phenylpiperidine

: 1448991-14-7
(S)-2-[(R)-azido(phenyl)methyl]-1-benzylpyrrolidine

Guidance literature:: With sodium azide; In dimethyl sulfoxide; N,N-dimethyl-formamide; at 55 ℃; for 2h; regioselective reaction; Microwave irradiation;
DOI:10.3987/COM-12-S(N)82

Reference yield:

: C₁₁H₁₄N₄

: 100-39-0
benzyl bromide

: 1448991-14-7
(S)-2-[(R)-azido(phenyl)methyl]-1-benzylpyrrolidine

Guidance literature:: C₁₁H₁₄N₄; With potassium carbonate; In N,N-dimethyl-formamide; for 0.166667h;

benzyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 10h;
DOI:10.1021/acs.joc.6b00218