Technology Process of C36H38O4
There total 4 articles about C36H38O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran; isopropyl alcohol;
at 75 ℃;
DOI:10.1021/ol402017x
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diisobutylaluminium hydride / tetrahydrofuran; n-heptane / 4.5 h / 20 °C
1.2: 20 °C
2.1: tetrahydrofuran; diethyl ether / 21 h / -80 °C
3.1: 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran; isopropyl alcohol / 75 °C
With
diisobutylaluminium hydride; 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran; diethyl ether; n-heptane; isopropyl alcohol;
3.1: |Stetter 1,4-Dicarbonyl Synthesis;
DOI:10.1021/ol402017x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran; diethyl ether / 21 h / -80 °C
2: 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran; isopropyl alcohol / 75 °C
With
3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran; diethyl ether; isopropyl alcohol;
2: |Stetter 1,4-Dicarbonyl Synthesis;
DOI:10.1021/ol402017x
