C₃₅H₃₃NO

Base Information

Chemical Name:C₃₅H₃₃NO
CAS No.:1373775-98-4
Molecular Formula:C₃₅H₃₃NO
Molecular Weight:483.653
Hs Code.:

Synonyms:C₃₅H₃₃NO

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Chemical Property of C₃₅H₃₃NO

Chemical Property:

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Technology Process of C₃₅H₃₃NO

There total 9 articles about C₃₅H₃₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 108-86-1,52753-63-6
bromobenzene

: 1373775-94-0
C₂₉H₂₉NO

: 1373775-98-4
C₃₅H₃₃NO

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; Trimethylacetic acid; In N,N-dimethyl-formamide; at 20 - 100 ℃; for 24h; Darkness; Inert atmosphere;
DOI:10.1021/ol300718x

Reference yield:

: 234111-16-1
2-((trimethylsilyl)ethynyl)cyclohex-1-ene-1-carbaldehyde

: 1373775-98-4
C₃₅H₃₃NO

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 1 h / -78 - 20 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: potassium fluoride / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere

4.1: copper(l) iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine / toluene / 24 h / 0 - 20 °C / Darkness; Inert atmosphere

5.1: palladium diacetate; potassium carbonate; triphenylphosphine; Trimethylacetic acid / N,N-dimethyl-formamide / 24 h / 20 - 100 °C / Darkness; Inert atmosphere

With potassium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; palladium diacetate; potassium carbonate; Dess-Martin periodane; magnesium; triphenylphosphine; Trimethylacetic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol300718x

Reference yield:

: C₁₈H₂₂OSi

: 1373775-98-4
C₃₅H₃₃NO

Guidance literature:: Multi-step reaction with 3 steps

1: potassium fluoride / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere

2: copper(l) iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine / toluene / 24 h / 0 - 20 °C / Darkness; Inert atmosphere

3: palladium diacetate; potassium carbonate; triphenylphosphine; Trimethylacetic acid / N,N-dimethyl-formamide / 24 h / 20 - 100 °C / Darkness; Inert atmosphere

With potassium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; palladium diacetate; potassium carbonate; triphenylphosphine; Trimethylacetic acid; In dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol300718x