2-acetamido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

Base Information

• Chemical Name: 2-acetamido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol
• CAS No.: 1643459-91-9
• Molecular Formula: C₁₈H₂₄N₂O₅
• Molecular Weight: 348.399

Synonyms:2-acetamido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

Chemical Property of 2-acetamido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

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Technology Process of 2-acetamido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

There total 2 articles about 2-acetamido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-azido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol (1643459-89-5) + acetic anhydride (108-24-7) → 2-acetamido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol (1643459-91-9)

Guidance literature:

With copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; water; for 0.666667h;

DOI:10.1039/c4ob00097h

Reference yield:

2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol (1643459-87-3) → 2-acetamido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol (1643459-91-9)

Guidance literature:

Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / 24 h / 0 °C / Inert atmosphere

2: zinc; acetic acid; copper(II) sulfate / tetrahydrofuran; water / 0.67 h

With boron trifluoride diethyl etherate; copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; water;

DOI:10.1039/c4ob00097h

Reference yield: 81.0%

2-acetamido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol (1643459-91-9) → 2-acetamido-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol (1643459-93-1)

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c4ob00097h

upstream raw materials:

2-azido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

acetic anhydride

2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

Downstream raw materials:

2-acetamido-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

2-acetamido-1,2,4-trideoxy-1,4-imino-D-lyxitol

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