2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

Base Information

Chemical Name:2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol
CAS No.:1643459-87-3
Molecular Formula:C₃₈H₃₆N₄O₂
Molecular Weight:580.729
Hs Code.:

Synonyms:2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

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Technology Process of 2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

There total 1 articles about 2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1643459-85-1
2-azido-3,5-di-O-benzhydryl-2-deoxy-1,4-di-O-methanesulfonyl-L-ribitol

: 100-46-9
benzylamine

: 1643459-87-3
2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

Guidance literature:: In toluene; at 80 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c4ob00097h

Reference yield: 70.0%

: 1643459-87-3
2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

: 108-24-7
acetic anhydride

: 1643459-89-5
2-azido-3,5-di-O-acetyl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

Guidance literature:: With boron trifluoride diethyl etherate; at 0 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c4ob00097h

Reference yield:

: 1643459-87-3
2-azido-3,5-di-O-benzhydryl-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

: 1643459-93-1
2-acetamido-N-benzyl-1,2,4-trideoxy-1,4-imino-D-lyxitol

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / 24 h / 0 °C / Inert atmosphere

2: zinc; acetic acid; copper(II) sulfate / tetrahydrofuran; water / 0.67 h

3: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; sodium methylate; copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; methanol; water;
DOI:10.1039/c4ob00097h