2-(2-benzoyl-4-methoxyphenyl)-1-(4-methoxyphenyl)-2-oxohydrazin-2-ium-1-ide

Base Information

Chemical Name:2-(2-benzoyl-4-methoxyphenyl)-1-(4-methoxyphenyl)-2-oxohydrazin-2-ium-1-ide
CAS No.:1456728-84-9
Molecular Formula:C₂₁H₁₈N₂O₄
Molecular Weight:362.385
Hs Code.:

Synonyms:2-(2-benzoyl-4-methoxyphenyl)-1-(4-methoxyphenyl)-2-oxohydrazin-2-ium-1-ide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-benzoyl-4-methoxyphenyl)-1-(4-methoxyphenyl)-2-oxohydrazin-2-ium-1-ide

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Technology Process of 2-(2-benzoyl-4-methoxyphenyl)-1-(4-methoxyphenyl)-2-oxohydrazin-2-ium-1-ide

There total 3 articles about 2-(2-benzoyl-4-methoxyphenyl)-1-(4-methoxyphenyl)-2-oxohydrazin-2-ium-1-ide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 100-52-7
benzaldehyde

: 1562-94-3,21650-70-4,51437-65-1
4,4'-dimethoxyazoxybenzene

: 1456728-84-9
2-(2-benzoyl-4-methoxyphenyl)-1-(4-methoxyphenyl)-2-oxohydrazin-2-ium-1-ide

Guidance literature:: With tert.-butylhydroperoxide; palladium(II) trifluoroacetate; In 1,2-dichloro-ethane; at 60 ℃; for 24h; regioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201400594

Reference yield: 76.0%

: 611-73-4
Benzoylformic acid

: 1562-94-3,21650-70-4,51437-65-1
4,4'-dimethoxyazoxybenzene

: 1456728-84-9
2-(2-benzoyl-4-methoxyphenyl)-1-(4-methoxyphenyl)-2-oxohydrazin-2-ium-1-ide

Guidance literature:: With dipotassium peroxodisulfate; palladium diacetate; In 1,2-dichloro-ethane; at 60 ℃; for 24h; regioselective reaction; Sealed tube;
DOI:10.1039/c3cc45492d

Reference yield: 75.0%

: 1562-94-3,21650-70-4,51437-65-1
4,4'-dimethoxyazoxybenzene

: 100-51-6,185532-71-2
benzyl alcohol

: 1456728-84-9
2-(2-benzoyl-4-methoxyphenyl)-1-(4-methoxyphenyl)-2-oxohydrazin-2-ium-1-ide

Guidance literature:: With tert.-butylhydroperoxide; palladium(II) trifluoroacetate; In 1,2-dichloro-ethane; at 100 ℃; for 20h; regioselective reaction; Sealed tube;
DOI:10.1039/c5ob00089k