(-)-(2R,3S)-2-mercaptomethyl-3-(2-methoxyphenoxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

Base Information

Chemical Name:(-)-(2R,3S)-2-mercaptomethyl-3-(2-methoxyphenoxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane
CAS No.:104128-58-7
Molecular Formula:C₂₁H₃₄O₈S
Molecular Weight:446.562
Hs Code.:

Synonyms:(-)-(2R,3S)-2-mercaptomethyl-3-(2-methoxyphenoxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

Suppliers and Price of (-)-(2R,3S)-2-mercaptomethyl-3-(2-methoxyphenoxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (-)-(2R,3S)-2-mercaptomethyl-3-(2-methoxyphenoxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (-)-(2R,3S)-2-mercaptomethyl-3-(2-methoxyphenoxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

There total 5 articles about (-)-(2R,3S)-2-mercaptomethyl-3-(2-methoxyphenoxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: Thiobenzoic acid S-[(2R,3S)-3-(2-methoxy-phenoxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl] ester

: 104128-58-7
(-)-(2R,3S)-2-mercaptomethyl-3-(2-methoxyphenoxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

Guidance literature:: With sodium hydroxide; In ethanol; for 1h; Ambient temperature;

Reference yield:

: 41024-91-3
penta(ethylene glycol) bis(p-toluenesulfonate)

: 104128-58-7
(-)-(2R,3S)-2-mercaptomethyl-3-(2-methoxyphenoxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

Guidance literature:: Multi-step reaction with 5 steps

1: 7.74 g / 60 percent NaH in oil / dimethylformamide / 19 h / 70 °C

2: 6.2 g / cc. HCl, H₂ / 5 percent Pd-C / ethanol / 1.5 h / Ambient temperature

3: 93 percent / pyridine / 48 h / -15 °C

4: 6.52 g / ethanol / 3 h / Heating

5: 60 percent / aq. 5 N NaOH / ethanol / 1 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; hydrogen; sodium hydride; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 104144-32-3
(2S,3S)-2-Benzyloxymethyl-3-(2-methoxy-phenoxymethyl)-1,4,7,10,13,16-hexaoxa-cyclooctadecane

: 104128-58-7
(-)-(2R,3S)-2-mercaptomethyl-3-(2-methoxyphenoxymethyl)-1,4,7,10,13,16-hexaoxacyclooctadecane

Guidance literature:: Multi-step reaction with 4 steps

1: 6.2 g / cc. HCl, H₂ / 5 percent Pd-C / ethanol / 1.5 h / Ambient temperature

2: 93 percent / pyridine / 48 h / -15 °C

3: 6.52 g / ethanol / 3 h / Heating

4: 60 percent / aq. 5 N NaOH / ethanol / 1 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; hydrogen; palladium on activated charcoal; In ethanol;