C₆H₅C₅H₃(CH₂OCH₂C₆H₃(OCH₂C₆H₃(N(C₆H₄)2)2)2)N

Base Information

• Chemical Name: C₆H₅C₅H₃(CH₂OCH₂C₆H₃(OCH₂C₆H₃(N(C₆H₄)2)2)2)N
• CAS No.: 1360816-37-0
• Molecular Formula: C₈₁H₅₇N₅O₃
• Molecular Weight: 1148.38
• Mol file: 1360816-37-0.mol

Synonyms:C₆H₅C₅H₃(CH₂OCH₂C₆H₃(OCH₂C₆H₃(N(C₆H₄)2)2)2)N

Chemical Property of C₆H₅C₅H₃(CH₂OCH₂C₆H₃(OCH₂C₆H₃(N(C₆H₄)2)2)2)N

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₆H₅C₅H₃(CH₂OCH₂C₆H₃(OCH₂C₆H₃(N(C₆H₄)2)2)2)N

There total 1 articles about C₆H₅C₅H₃(CH₂OCH₂C₆H₃(OCH₂C₆H₃(N(C₆H₄)2)2)2)N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4-(hydroxymethyl)-2-phenylpyridine (4634-12-2) + C69H47BrN4O2 (913332-10-2) → C6H5C5H3(CH2OCH2C6H3(OCH2C6H3(N(C6H4)2)2)2)N (1360816-37-0)

Guidance literature:

4-(hydroxymethyl)-2-phenylpyridine; With sodium hydride; In N,N-dimethyl-formamide; for 0.5h; Cooling with ice;

C₆₉H₄₇BrN₄O₂; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c1dt11716e

Reference yield:

iridium(III) chloride trihydrate + C6H5C5H3(CH2OCH2C6H3(OCH2C6H3(N(C6H4)2)2)2)N (1360816-37-0) → 4C6H4C5H3(CH2OCH2C6H3(OCH2C6H3(N(C6H4)2)2)2)N(1-)*2Ir(3+)*2Cl(1-)=[(C6H4C5H3(CH2OCH2C6H3(OCH2C6H3(N(C6H4)2)2)2)N)2IrCl]2

Guidance literature:

In 2-methoxy-ethanol; water; Ir salt and ligand (2.5 equiv.) added to 2-methoxyethanol/H2O (3/1), mixt. refluxed for 36 h; cooled to room temp., soln. filtered through Celite, ppt. washed (H2O, ether, hexane), dried under vac.;

DOI:10.1039/c1dt11716e

upstream raw materials:

4-(hydroxymethyl)-2-phenylpyridine

C₆₉H₄₇BrN₄O₂

Refernces