Diethyl N-[2-(2-chlorophenyl)ethenyl]phosphoramidate

Base Information

Chemical Name:Diethyl N-[2-(2-chlorophenyl)ethenyl]phosphoramidate
CAS No.:86423-59-8
Molecular Formula:C₁₂H₁₇ClNO₃P
Molecular Weight:289.699
Hs Code.:
DSSTox Substance ID:DTXSID201217660

Synonyms:DTXSID201217660;Diethyl N-[2-(2-chlorophenyl)ethenyl]phosphoramidate;86423-59-8

Suppliers and Price of Diethyl N-[2-(2-chlorophenyl)ethenyl]phosphoramidate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diethyl N-[2-(2-chlorophenyl)ethenyl]phosphoramidate

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:289.0634581
Heavy Atom Count:18
Complexity:302

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(NC=CC1=CC=CC=C1Cl)OCC

Technology Process of Diethyl N-[2-(2-chlorophenyl)ethenyl]phosphoramidate

There total 3 articles about Diethyl N-[2-(2-chlorophenyl)ethenyl]phosphoramidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 86423-59-8
Diethyl N-<β-(o-chlorophenyl)-vinyl>phosphoramidate

Guidance literature:

Reference yield:

: 86052-27-9
Diethyl N-o-chlorobenzylideneaminomethylphosphonate

: 86423-59-8
Diethyl N-<β-(o-chlorophenyl)-vinyl>phosphoramidate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 45 ℃; for 2h; Yield given;
DOI:10.1055/s-1987-27902

Reference yield:

: 89-98-5
2-chloro-benzaldehyde

: 86423-59-8
Diethyl N-<β-(o-chlorophenyl)-vinyl>phosphoramidate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / toluene / 0.5 h / Ambient temperature

2: NaH / tetrahydrofuran / 2 h / 45 °C

With sodium hydride; In tetrahydrofuran; toluene;
DOI:10.1055/s-1987-27902