Methyl 4-[N-methyl-N-(2-methoxy-4-nitrobenzyloxycarbonyl)amino]phenylacetate

Base Information

Chemical Name:Methyl 4-[N-methyl-N-(2-methoxy-4-nitrobenzyloxycarbonyl)amino]phenylacetate
CAS No.:251643-29-5
Molecular Formula:C₁₉H₂₀N₂O₇
Molecular Weight:388.377
Hs Code.:

Synonyms:Methyl 4-[N-methyl-N-(2-methoxy-4-nitrobenzyloxycarbonyl)amino]phenylacetate

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Chemical Property of Methyl 4-[N-methyl-N-(2-methoxy-4-nitrobenzyloxycarbonyl)amino]phenylacetate

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Technology Process of Methyl 4-[N-methyl-N-(2-methoxy-4-nitrobenzyloxycarbonyl)amino]phenylacetate

There total 6 articles about Methyl 4-[N-methyl-N-(2-methoxy-4-nitrobenzyloxycarbonyl)amino]phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 251643-16-0
methyl 2-(4-(methylamino)phenyl)acetate

: C₉H₈ClNO₅

: 251643-29-5
Methyl 4-[N-methyl-N-(2-methoxy-4-nitrobenzyloxycarbonyl)amino]phenylacetate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1039/a904067f

Reference yield:

: 76143-33-4
5-(methoxycarbonyl)-2-nitrobenzoic acid

: 251643-29-5
Methyl 4-[N-methyl-N-(2-methoxy-4-nitrobenzyloxycarbonyl)amino]phenylacetate

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / dimethylformamide / 3 h / Heating

2: tetrahydrofuran / 0.5 h / -10 °C

3: BH₃*DMS / tetrahydrofuran / 1 h / 20 °C

4: CS₂CO₃ / dimethylformamide / 16 h / 20 °C

With thionyl chloride; dimethylsulfide borane complex; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; 1: Substitution / 2: Formylation / 3: Reduction / 4: Acylation;
DOI:10.1039/a904067f

Reference yield:

: 39106-79-1
methyl 2-methoxy-4-nitrobenzoate

: 251643-29-5
Methyl 4-[N-methyl-N-(2-methoxy-4-nitrobenzyloxycarbonyl)amino]phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / DIBAL-H / tetrahydrofuran; toluene / 0.25 h / 2 °C

2: benzene; tetrahydrofuran / 16 h / 20 °C

3: CS₂CO₃ / dimethylformamide / 16 h / 20 °C

With diisobutylaluminium hydride; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; benzene; 1: Reduction / 2: Substitution / 3: Acylation;
DOI:10.1039/a904067f