(Z)-1-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-3-(2-hydroxyethyl)-3-methyltriaz-1-ene 2-oxide

Base Information

Chemical Name:(Z)-1-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-3-(2-hydroxyethyl)-3-methyltriaz-1-ene 2-oxide
CAS No.:1609495-40-0
Molecular Formula:C₂₁H₂₄ClN₃O₇
Molecular Weight:465.89
Hs Code.:

Synonyms:(Z)-1-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-3-(2-hydroxyethyl)-3-methyltriaz-1-ene 2-oxide

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Chemical Property of (Z)-1-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-3-(2-hydroxyethyl)-3-methyltriaz-1-ene 2-oxide

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Technology Process of (Z)-1-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-3-(2-hydroxyethyl)-3-methyltriaz-1-ene 2-oxide

There total 3 articles about (Z)-1-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-3-(2-hydroxyethyl)-3-methyltriaz-1-ene 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: (Z)-1-hydroxy-3-(2-hydroxyethyl)-3-methyltriaz-1-ene 2-oxide sodium salt

: 1609495-38-6
iodomethyl 2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoate

: 1609495-40-0
(Z)-1-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-3-(2-hydroxyethyl)-3-methyltriaz-1-ene 2-oxide

Guidance literature:: In hexane; N,N-dimethyl-formamide; at 20 ℃; for 1.06667h; Cooling with ice;

Reference yield:

: 1094101-30-0
chloromethyl 2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoate

: 1609495-40-0
(Z)-1-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-3-(2-hydroxyethyl)-3-methyltriaz-1-ene 2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide / acetone / 6.17 h / 20 - 50 °C

2: N,N-dimethyl-formamide; hexane / 1.07 h / 20 °C / Cooling with ice

With sodium iodide; In hexane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 42017-89-0
fenofibric acid

: 1609495-40-0
(Z)-1-((2-(4-(4-chlorobenzoyl)phenoxy)-2-methylpropanoyloxy) methoxy)-3-(2-hydroxyethyl)-3-methyltriaz-1-ene 2-oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate; tetra(n-butyl)ammonium hydrogensulfate / water / 0.25 h / 20 °C

1.2: 20 °C / Cooling with ice

2.1: sodium iodide / acetone / 6.17 h / 20 - 50 °C

3.1: N,N-dimethyl-formamide; hexane / 1.07 h / 20 °C / Cooling with ice

With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; sodium iodide; In hexane; water; N,N-dimethyl-formamide; acetone;