C₅₆H₆₃N₅O₁₃

Base Information

Chemical Name:C₅₆H₆₃N₅O₁₃
CAS No.:843663-76-3
Molecular Formula:C₅₆H₆₃N₅O₁₃
Molecular Weight:1014.14
Hs Code.:

C<sub>56</sub>H<sub>63</sub>N<sub>5</sub>O<sub>13</sub>

Synonyms:C₅₆H₆₃N₅O₁₃

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Chemical Property of C₅₆H₆₃N₅O₁₃

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Technology Process of C₅₆H₆₃N₅O₁₃

There total 13 articles about C₅₆H₆₃N₅O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 405519-78-0
4-bromo-3-[2-(tert-butyl-diphenyl-silanyloxymethyl)-oxazol-5-yl]-1-methoxymethyl-1H-indole

: 843663-76-3
C₅₆H₆₃N₅O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: 92 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C

2.1: 93 percent / Et₃N / CH₂Cl₂ / 0.33 h / 0 °C

3.1: 83 percent / Pd(diphenylphosphinoferrocene)Cl₂*CH₂Cl₂; K₂CO₃ / 1,2-dimethoxy-ethane / 12 h / Heating

4.1: 93 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.33 h / 25 °C

5.1: 87 percent / Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 1 h / 25 °C

6.1: 87 percent / dimethylsulfoxide / 0.17 h / 25 °C

7.1: SmI₂; hexamethylphosphoramide / tetrahydrofuran / 0.75 h / 25 °C

7.2: 41 percent / 1-hydroxy-1H-benzotriazole hydrate; 3-(3-dimethylaminopropyl)-1-ethylcarbodiimide / dimethylformamide / 30 h / 25 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; dimethyl sulfoxide; 3.1: Suzuki coupling;
DOI:10.1021/ja040091q

Reference yield:

: 760979-81-5
[5-(4-bromo-1-methoxymethyl-1H-indol-3-yl)-oxazol-2-yl]-methanol

: 843663-76-3
C₅₆H₆₃N₅O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 93 percent / Et₃N / CH₂Cl₂ / 0.33 h / 0 °C

2.1: 83 percent / Pd(diphenylphosphinoferrocene)Cl₂*CH₂Cl₂; K₂CO₃ / 1,2-dimethoxy-ethane / 12 h / Heating

3.1: 93 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.33 h / 25 °C

4.1: 87 percent / Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 1 h / 25 °C

5.1: 87 percent / dimethylsulfoxide / 0.17 h / 25 °C

6.1: SmI₂; hexamethylphosphoramide / tetrahydrofuran / 0.75 h / 25 °C

6.2: 41 percent / 1-hydroxy-1H-benzotriazole hydrate; 3-(3-dimethylaminopropyl)-1-ethylcarbodiimide / dimethylformamide / 30 h / 25 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; dimethyl sulfoxide; 2.1: Suzuki coupling;
DOI:10.1021/ja040091q

Reference yield:

: 760980-01-6
4-bromo-3-[2-(tert-butyl-dimethyl-silanyloxymethyl)-oxazol-5-yl]-1-methoxymethyl-1H-indole

: 843663-76-3
C₅₆H₆₃N₅O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: 83 percent / Pd(diphenylphosphinoferrocene)Cl₂*CH₂Cl₂; K₂CO₃ / 1,2-dimethoxy-ethane / 12 h / Heating

2.1: 93 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.33 h / 25 °C

3.1: 87 percent / Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 1 h / 25 °C

4.1: 87 percent / dimethylsulfoxide / 0.17 h / 25 °C

5.1: SmI₂; hexamethylphosphoramide / tetrahydrofuran / 0.75 h / 25 °C

5.2: 41 percent / 1-hydroxy-1H-benzotriazole hydrate; 3-(3-dimethylaminopropyl)-1-ethylcarbodiimide / dimethylformamide / 30 h / 25 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; dimethyl sulfoxide; 1.1: Suzuki coupling;
DOI:10.1021/ja040091q