Technology Process of bis[(2-phenylthiolato)phenylphosphino-S,S',P]-tris(4-methylphenyl)phosphine-palladium(II)
There total 1 articles about bis[(2-phenylthiolato)phenylphosphino-S,S',P]-tris(4-methylphenyl)phosphine-palladium(II) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
NEt3;
In
dichloromethane;
byproducts: P(C6H4-4-Me)3; under N2 using standard Schlenk technique; soln. of bis(2-phenylthiol)phenylphosphine (1 equiv.) and NEt3 (1.227 mmol) added to soln. of Pt complex (0.613 mmol); stirred (24 h); filtered off; evapd. (vac.); recrystd. from CH2Cl2/MeOH double layer system; elem. anal.;
DOI:10.1016/j.ica.2006.10.029