2-aminophenylboronic acid (-)-1,2-dicyclohexyl-1,2-ethanediol ester

Base Information

Chemical Name:2-aminophenylboronic acid (-)-1,2-dicyclohexyl-1,2-ethanediol ester
CAS No.:616227-07-7
Molecular Formula:C₂₀H₃₀BNO₂
Molecular Weight:327.275
Hs Code.:

Synonyms:2-aminophenylboronic acid (-)-1,2-dicyclohexyl-1,2-ethanediol ester

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Chemical Property of 2-aminophenylboronic acid (-)-1,2-dicyclohexyl-1,2-ethanediol ester

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Technology Process of 2-aminophenylboronic acid (-)-1,2-dicyclohexyl-1,2-ethanediol ester

There total 3 articles about 2-aminophenylboronic acid (-)-1,2-dicyclohexyl-1,2-ethanediol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 5570-18-3
2-aminophenylboronic acid

: 120850-92-2
(1R,2R)-1,2-dicyclohexyl-1,2-ethanediol

: 616227-07-7
2-aminophenylboronic acid (-)-1,2-dicyclohexyl-1,2-ethanediol ester

Guidance literature:: In tetrahydrofuran;
DOI:10.1016/S0022-328X(03)00400-5

Reference yield:

: 5570-19-4
2-nitrophenylboronic acid

: 616227-07-7
2-aminophenylboronic acid (-)-1,2-dicyclohexyl-1,2-ethanediol ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol

2: 93 percent / tetrahydrofuran

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1016/S0022-328X(03)00400-5

Reference yield:

: 98-80-6
phenylboronic acid

: 616227-07-7
2-aminophenylboronic acid (-)-1,2-dicyclohexyl-1,2-ethanediol ester

Guidance literature:: Multi-step reaction with 3 steps

1: HNO₃; Ac₂O; urea

2: H₂ / Pd/C / ethanol

3: 93 percent / tetrahydrofuran

With hydrogen; nitric acid; acetic anhydride; urea; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1016/S0022-328X(03)00400-5