dimethyl N-((cis-3-acetyl-2,2-dimethylcyclobutyl)thioethanoyl)-N-benzylphosphoramidate

Base Information

Chemical Name:dimethyl N-((cis-3-acetyl-2,2-dimethylcyclobutyl)thioethanoyl)-N-benzylphosphoramidate
CAS No.:130012-59-8
Molecular Formula:C₁₉H₂₈NO₄PS
Molecular Weight:397.475
Hs Code.:

Synonyms:dimethyl N-((cis-3-acetyl-2,2-dimethylcyclobutyl)thioethanoyl)-N-benzylphosphoramidate

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Chemical Property of dimethyl N-((cis-3-acetyl-2,2-dimethylcyclobutyl)thioethanoyl)-N-benzylphosphoramidate

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Technology Process of dimethyl N-((cis-3-acetyl-2,2-dimethylcyclobutyl)thioethanoyl)-N-benzylphosphoramidate

There total 5 articles about dimethyl N-((cis-3-acetyl-2,2-dimethylcyclobutyl)thioethanoyl)-N-benzylphosphoramidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17879-35-5,52305-34-7,61376-92-9,61826-55-9,64396-97-0,127062-09-3,473-72-3
cis-pinonic acid

: 130012-59-8
dimethyl N-((cis-3-acetyl-2,2-dimethylcyclobutyl)thioethanoyl)-N-benzylphosphoramidate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / pyridine, thionyl chloride / diethyl ether / 0 deg C (15 min.) to room temperature

2: 1.) sodium hydride / 1.) THF, reflux, 2 h, 2.) 0 deg C to room temperature, 15-30 min.

3: CCl₄ / Heating

With pyridine; thionyl chloride; sodium hydride; In tetrachloromethane; diethyl ether;
DOI:10.1021/jo00312a012

Reference yield:

: 130062-20-3
cis(+/-)-3-acetyl-2,2-dimethylcyclobutylacetic acid chloride

: 130012-59-8
dimethyl N-((cis-3-acetyl-2,2-dimethylcyclobutyl)thioethanoyl)-N-benzylphosphoramidate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) THF, reflux, 2 h, 2.) 0 deg C to room temperature, 15-30 min.

2: CCl₄ / Heating

With sodium hydride; In tetrachloromethane;
DOI:10.1021/jo00312a012

Reference yield:

: 130012-35-0
dimethyl N-benzylphosphoramidothionate

: 130012-59-8
dimethyl N-((cis-3-acetyl-2,2-dimethylcyclobutyl)thioethanoyl)-N-benzylphosphoramidate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) THF, reflux, 2 h, 2.) 0 deg C to room temperature, 15-30 min.

2: CCl₄ / Heating

With sodium hydride; In tetrachloromethane;
DOI:10.1021/jo00312a012