(-)-(1R,5S)-5-(acetoxymethyl)-3-benzyl-1-<((methoxymethyl)oxy)methyl>-9-methylene-3-azabicyclo<3.3.1>nonane

Base Information

Chemical Name:(-)-(1R,5S)-5-(acetoxymethyl)-3-benzyl-1-<((methoxymethyl)oxy)methyl>-9-methylene-3-azabicyclo<3.3.1>nonane
CAS No.:124022-33-9
Molecular Formula:C₂₂H₃₁NO₄
Molecular Weight:373.492
Hs Code.:

Synonyms:(-)-(1R,5S)-5-(acetoxymethyl)-3-benzyl-1-<((methoxymethyl)oxy)methyl>-9-methylene-3-azabicyclo<3.3.1>nonane

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Chemical Property of (-)-(1R,5S)-5-(acetoxymethyl)-3-benzyl-1-<((methoxymethyl)oxy)methyl>-9-methylene-3-azabicyclo<3.3.1>nonane

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Technology Process of (-)-(1R,5S)-5-(acetoxymethyl)-3-benzyl-1-<((methoxymethyl)oxy)methyl>-9-methylene-3-azabicyclo<3.3.1>nonane

There total 2 articles about (-)-(1R,5S)-5-(acetoxymethyl)-3-benzyl-1-<((methoxymethyl)oxy)methyl>-9-methylene-3-azabicyclo<3.3.1>nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113161-31-2
3-benzyl-1,5-(dihydroxymethyl)-9-methylene-3-azabicyclo<3.3.1>nonane

: 124022-33-9
(-)-(1R,5S)-5-(acetoxymethyl)-3-benzyl-1-<((methoxymethyl)oxy)methyl>-9-methylene-3-azabicyclo<3.3.1>nonane

Guidance literature:: Multi-step reaction with 2 steps

1: 1 percent / Candidia cylindracea lipase-type VII / benzene / 11 h / 28 °C

2: 1.) Celite, Candida cylindracea lipase-type VII, 2.) i-Pr₂NEt / 1.) H₂O, isooctane, 35 deg C, 2 d, 2.) CH₂Cl₂, RT, 20 h

With Candida cylindracea lipase-type VII; Candidia cylindracea lipase-type VII; Celite; N-ethyl-N,N-diisopropylamine; In benzene;
DOI:10.1021/ja00159a042

Reference yield:

: 124022-28-2
1,5-(diacetoxymethyl)-3-benzyl-9-methylene-3-azabicyclo<3.3.1>nonane

: 107-30-2
chloromethyl methyl ether

: 124022-33-9
(-)-(1R,5S)-5-(acetoxymethyl)-3-benzyl-1-<((methoxymethyl)oxy)methyl>-9-methylene-3-azabicyclo<3.3.1>nonane

Guidance literature:: With Candida cylindracea lipase-type VII; Celite; N-ethyl-N,N-diisopropylamine; Multistep reaction; 1.) H₂O, isooctane, 35 deg C, 2 d, 2.) CH₂Cl₂, RT, 20 h;
DOI:10.1021/ja00159a042