N,N’-bis-(2,6-diisopropyl,4-nitrophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

Base Information

Chemical Name:N,N’-bis-(2,6-diisopropyl,4-nitrophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene
CAS No.:849472-27-1
Molecular Formula:C₂₈H₃₈N₄O₄
Molecular Weight:494.634
Hs Code.:

Synonyms:N,N’-bis-(2,6-diisopropyl,4-nitrophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N’-bis-(2,6-diisopropyl,4-nitrophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

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Technology Process of N,N’-bis-(2,6-diisopropyl,4-nitrophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

There total 1 articles about N,N’-bis-(2,6-diisopropyl,4-nitrophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 431-03-8
dimethylglyoxal

: 163704-72-1
4-nitro-2,6-diisopropyl aniline

: 849472-27-1
N,N’-bis-(2,6-diisopropyl,4-nitrophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

Guidance literature:: With toluene-4-sulfonic acid; trimethyl orthoformate; In methanol; for 8h;
DOI:10.1016/j.molcata.2016.07.045

Reference yield: 74.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 849472-27-1
N,N’-bis-(2,6-diisopropyl,4-nitrophenyl)-2,3-dimethyl-1,4-diaza-1,3-butadiene

: 849472-21-5
[(2,6-(i-Pr)2-4-NO₂C₆H₂N=C(Me)C(Me)=NC₆H₂-2,6-(i-Pr)2-4-NO₂)PdMeCl]

Guidance literature:: With tetramethylstannane; In dichloromethane; Me4Sn was added to soln. of Pd complex in CH2Cl2 at -35°C under Ar; mixt. was stirred at -35°C for 2.5 h; soln. of ligand in CH2Cl2 was added; mixt. was kept at low temp. for 15 min; warmed to room temp.; stired overnight; chromd. (silica gel, hexane/CH2Cl2/EtOAc, 5/4/1); concd.; dried (vac.); elem. anal.;
DOI:10.1021/om048988j