(S)-Allyl-phosphonic acid benzyl ester (S)-1-trityloxymethyl-allyl ester

Base Information

Chemical Name:(S)-Allyl-phosphonic acid benzyl ester (S)-1-trityloxymethyl-allyl ester
CAS No.:863012-07-1
Molecular Formula:C₃₃H₃₃O₄P
Molecular Weight:524.596
Hs Code.:

Synonyms:(S)-Allyl-phosphonic acid benzyl ester (S)-1-trityloxymethyl-allyl ester

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Chemical Property of (S)-Allyl-phosphonic acid benzyl ester (S)-1-trityloxymethyl-allyl ester

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Technology Process of (S)-Allyl-phosphonic acid benzyl ester (S)-1-trityloxymethyl-allyl ester

There total 2 articles about (S)-Allyl-phosphonic acid benzyl ester (S)-1-trityloxymethyl-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129940-50-7
(S)-tritylglycidol

: 863012-07-1
(S)-Allyl-phosphonic acid benzyl ester (S)-1-trityloxymethyl-allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / BuLi / tetrahydrofuran

2: 57 percent / BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

3: BuLi / 1,2-dimethoxy-ethane; hexane / -50 - 20 °C

With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; hexane;
DOI:10.1021/jo0505122

Reference yield:

: 403985-96-6
(S)-1-(triphenylmethoxy)-3-buten-2-ol

: 863012-07-1
(S)-Allyl-phosphonic acid benzyl ester (S)-1-trityloxymethyl-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

2: BuLi / 1,2-dimethoxy-ethane; hexane / -50 - 20 °C

With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; hexane;
DOI:10.1021/jo0505122