(Z)-4,4,5,5-tetramethyl-2-(1-methyl-3-phenylmethoxy-1-propenyl)-1,3,2-dioxaborolane

Base Information

Chemical Name:(Z)-4,4,5,5-tetramethyl-2-(1-methyl-3-phenylmethoxy-1-propenyl)-1,3,2-dioxaborolane
CAS No.:791845-45-9
Molecular Formula:C₁₇H₂₅BO₃
Molecular Weight:288.195
Hs Code.:

Synonyms:(Z)-4,4,5,5-tetramethyl-2-(1-methyl-3-phenylmethoxy-1-propenyl)-1,3,2-dioxaborolane

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Chemical Property of (Z)-4,4,5,5-tetramethyl-2-(1-methyl-3-phenylmethoxy-1-propenyl)-1,3,2-dioxaborolane

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Technology Process of (Z)-4,4,5,5-tetramethyl-2-(1-methyl-3-phenylmethoxy-1-propenyl)-1,3,2-dioxaborolane

There total 8 articles about (Z)-4,4,5,5-tetramethyl-2-(1-methyl-3-phenylmethoxy-1-propenyl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 4885-07-8
((but-2-yn-1-yloxy)methyl)benzene

: 73183-34-3
bis(pinacol)diborane

: 791845-45-9
(Z)-4,4,5,5-tetramethyl-2-(1-methyl-3-phenylmethoxy-1-propenyl)-1,3,2-dioxaborolane

Guidance literature:: With NaOC(CH₃)3; CuCl; P(C₆H₁₁)3; In toluene; B2(O2C2(CH3)4)2 reacted with CH3C2CH2OCH2C6H5 in the presence of CuCl, NaOC(CH3)3, P(C6H11)3, and CH3OH in toluene at room temp.; chromd.; >98/<2 ratio of regioisomers;
DOI:10.1021/ja300627s

Reference yield:

: 73183-34-3
bis(pinacol)diborane

: ((buta-2,3-dien-1-yloxy)methyl)benzene

: 791845-45-9
(Z)-4,4,5,5-tetramethyl-2-(1-methyl-3-phenylmethoxy-1-propenyl)-1,3,2-dioxaborolane

: 2-(4-(benzyloxy)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With copper(II) sulfate; triphenylphosphine; benzylamine; In water; at 20 ℃; for 3h; Overall yield = 53 percent; Inert atmosphere;
DOI:10.1039/d0nj02010a

Reference yield:

: C₂₃H₃₈B₂O₆

: 791845-45-9
(Z)-4,4,5,5-tetramethyl-2-(1-methyl-3-phenylmethoxy-1-propenyl)-1,3,2-dioxaborolane

: 2-(4-(benzyloxy)but-1-en-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 65 ℃; for 24h; Overall yield = 0.117 g; stereoselective reaction;
DOI:10.1021/jo500773t