Ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Base Information

Chemical Name:Ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate
CAS No.:1415043-07-0
Molecular Formula:C₂₅H₂₅FN₂O₅S
Molecular Weight:484.548
Hs Code.:

Synonyms:Ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

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Chemical Property of Ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

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Technology Process of Ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

There total 5 articles about Ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1004293-27-9
2-[(4-fluorophenyl)sulfonyl]benzaldehyde

: 1415042-82-8
tert-butyl 1-(2-ethoxy-2-oxoethyl)-2-methyl-4-oxo-1,4,6,7-tetrahydro-5H-pyrrolo[3,2-c]pyridine-5-carboxylate

: 1415043-07-0
Ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Guidance literature:: With water; hydrogen iodide; hypophosphorous acid; acetic anhydride; at 20 ℃; for 2h;

Reference yield:

: 643763-14-8
2-[(4-fluorophenyl)sulfanyl]benzaldehyde

: 1415043-07-0
Ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Cooling with acetone-dry ice

2: acetic anhydride; hypophosphorous acid; water; hydrogen iodide / 2 h / 20 °C

With water; hydrogen iodide; hypophosphorous acid; acetic anhydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

Reference yield:

: 845267-78-9
tert-butyl 2,4-dioxopiperidine-1-carboxylate

: 1415043-07-0
Ethyl (3-{2-[(4-fluorophenyl)sulfonyl]benzyl}-2-methyl-4-oxo-4,5,6,7-tetrahydro-1H-pyrrolo[3,2-c]pyridin-1-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / chloroform / 20 °C

2: sodium acetate / ethanol / 20 °C

3: acetic anhydride; hypophosphorous acid; water; hydrogen iodide / 2 h / 20 °C

With water; hydrogen iodide; sodium acetate; hypophosphorous acid; acetic anhydride; potassium carbonate; In ethanol; chloroform;