C₂₈H₂₆N₂O₄

Base Information

Chemical Name:C₂₈H₂₆N₂O₄
CAS No.:616890-15-4
Molecular Formula:C₂₈H₂₆N₂O₄
Molecular Weight:454.525
Hs Code.:

C<sub>28</sub>H<sub>26</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₈H₂₆N₂O₄

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Chemical Property of C₂₈H₂₆N₂O₄

Chemical Property:

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Technology Process of C₂₈H₂₆N₂O₄

There total 8 articles about C₂₈H₂₆N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 582315-05-7
(3S,3''S,3'aR,7'aR)-1-benzyl-1''-methyl-2',2'-dimethyl-3'a,4',7',7'a-tetrahydrospiro[3H-indole-3,5'(6'H)-[1,3]benzodioxole-6'-3''-[3H]indole]-2,2''-(1H,1''H)-dione

: 616890-15-4
C₂₈H₂₆N₂O₄

Guidance literature:: With camphor-10-sulfonic acid; In methanol; dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/S0040-4020(03)00855-X

Reference yield:

: 1217-89-6
1-benzylisatin

: 616890-15-4
C₂₈H₂₆N₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: 76 percent / AcOH; HCl / 6 h / 110 °C

2.1: 97 percent / Cs₂CO₃ / dimethylformamide / 24 h / 20 °C

3.1: 88 percent / H₂ / PtO₂ / ethyl acetate / 20 °C / 760 Torr

4.1: LHMDS / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.5 h / -40 °C

4.2: 75 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / 13 h / -35 - 20 °C

5.1: 98 percent / camphorsulfonic acid / methanol; CH₂Cl₂ / 3 h / 20 °C

With hydrogenchloride; camphor-10-sulfonic acid; hydrogen; caesium carbonate; acetic acid; lithium hexamethyldisilazane; platinum(IV) oxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(03)00855-X

Reference yield:

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 616890-15-4
C₂₈H₂₆N₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: 99 percent / NaH / dimethylformamide / 0.25 h

2.1: 76 percent / AcOH; HCl / 6 h / 110 °C

3.1: 97 percent / Cs₂CO₃ / dimethylformamide / 24 h / 20 °C

4.1: 88 percent / H₂ / PtO₂ / ethyl acetate / 20 °C / 760 Torr

5.1: LHMDS / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.5 h / -40 °C

5.2: 75 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / 13 h / -35 - 20 °C

6.1: 98 percent / camphorsulfonic acid / methanol; CH₂Cl₂ / 3 h / 20 °C

With hydrogenchloride; camphor-10-sulfonic acid; hydrogen; sodium hydride; caesium carbonate; acetic acid; lithium hexamethyldisilazane; platinum(IV) oxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(03)00855-X