C₆₂H₈₆N₂O₁₅Si

Base Information

Chemical Name:C₆₂H₈₆N₂O₁₅Si
CAS No.:245736-73-6
Molecular Formula:C₆₂H₈₆N₂O₁₅Si
Molecular Weight:1127.45
Hs Code.:

C<sub>62</sub>H<sub>86</sub>N<sub>2</sub>O<sub>15</sub>Si

Synonyms:C₆₂H₈₆N₂O₁₅Si

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Chemical Property of C₆₂H₈₆N₂O₁₅Si

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Technology Process of C₆₂H₈₆N₂O₁₅Si

There total 38 articles about C₆₂H₈₆N₂O₁₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 245736-72-5
C₆₂H₈₈N₂O₁₆Si

: 245736-73-6
C₆₂H₈₆N₂O₁₅Si

Guidance literature:: With N-ethyl-N,N-diisopropylamine; m-chlorophenyl isocyanate; In benzene; at 90 ℃;
DOI:10.1021/ja990789h

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 245736-73-6
C₆₂H₈₆N₂O₁₅Si

Guidance literature:: Multi-step reaction with 21 steps

1: NaH / dimethylformamide; tetrahydrofuran

2: HCl / methanol; diethyl ether / 0 °C

3: (COCl)2, DMSO, i-Pr₂NEt / -78 - -30 °C

4: 73 percent / TiCl₂(O-i-Pr)2 / CH₂Cl₂ / -78 - 0 °C

5: Et₂BOMe, NaBH₄ / tetrahydrofuran; methanol / -78 °C

6: HCl

7: DIBAL-H / CH₂Cl₂ / -78 °C

8: 1.) Bu₂BOTf, i-Pr₂NEt / 1.) CH₂Cl₂, 0 deg C, 2.) CH₂Cl₂, -78 deg C

9: 100 percent / (COCl)2, DMSO, i-Pr₂NEt / -78 - 0 °C

10: 82 percent / TsOH / acetonitrile / -22 °C

11: 100 percent / (COCl)2, DMSO, Et₃N / -78 - 0 °C

12: LDA / 1 h / -78 °C

13: LiOOH / tetrahydrofuran; dimethylformamide; H₂O / 0 - 23 °C

14: aq. OsO₄, NMO / tetrahydrofuran; 2-methyl-propan-2-ol

15: aq. NaIO₄, NaHCO₃ / tetrahydrofuran; 2-methyl-propan-2-ol

16: 1.) Et₃N, 2.) Et₃NHOAc

17: 1.) c-hex2BCl, Me₂NEt / 1.) Et₂O, 0 deg C, 2.) Et₂O, from -78 deg C to 0 deg C

18: imidazole / CH₂Cl₂

19: Et₃NHOAc

20: (2,4,6-Cl₃PhCO)2O, i-Pr₂NEt, DMAP / benzene

21: 68 percent / 3-ClPhNCO, i-Pr₂NEt / benzene / 90 °C

With 1H-imidazole; hydrogenchloride; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; titanium(IV) dichlorodiisopropylate; oxalyl dichloride; lithium hydroperoxide; N,N-dimethyl-ethanamine; di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; dicyclohexylboron chloride; triethylammonium acetate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; m-chlorophenyl isocyanate; lithium diisopropyl amide; 2,4,6-trichlorobenzoic anhydride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1021/ja990789h

Reference yield:

: 136546-79-7
<4S,3(2R)>-4-benzyl-3-<4-(tert-butoxycarbonyl)-2-methylbutanoyl>-2-oxazolidinone

: 245736-73-6
C₆₂H₈₆N₂O₁₅Si

Guidance literature:: Multi-step reaction with 14 steps

1: LiBH₄ / methanol; tetrahydrofuran / 0 °C

2: (COCl)2, DMSO, Et₃N / -78 - 0 °C

3: Ph₃P / CH₂Cl₂ / 0 °C

4: 99 percent / TFA / CH₂Cl₂

5: 83 percent / n-BuLi / tetrahydrofuran / -78 °C

6: (COCl)2 / benzene

7: n-BuLi / tetrahydrofuran / 0 °C

8: 1.) Bu₂BOTf, Et₃N / 1.) CH₂Cl₂, 0 deg C, 2.) CH₂Cl₂, -78 deg C

9: 95 percent / SO₃*pyr, i-Pr₂NEt / dimethylsulfoxide; CH₂Cl₂ / -15 °C

10: 1.) c-hex2BCl, Me₂NEt / 1.) Et₂O, 0 deg C, 2.) Et₂O, from -78 deg C to 0 deg C

11: imidazole / CH₂Cl₂

12: Et₃NHOAc

13: (2,4,6-Cl₃PhCO)2O, i-Pr₂NEt, DMAP / benzene

14: 68 percent / 3-ClPhNCO, i-Pr₂NEt / benzene / 90 °C

With 1H-imidazole; dmap; lithium borohydride; n-butyllithium; oxalyl dichloride; pyridine-SO₃ complex; N,N-dimethyl-ethanamine; di-n-butylboryl trifluoromethanesulfonate; dicyclohexylboron chloride; triethylammonium acetate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; m-chlorophenyl isocyanate; 2,4,6-trichlorobenzoic anhydride; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; benzene;
DOI:10.1021/ja990789h