trideuteriomethyl O-(3,4-di-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-mannopyranoside

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Chemical Name:trideuteriomethyl O-(3,4-di-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-mannopyranoside
CAS No.:105608-14-8
Molecular Formula:C₄₈H₅₄O₁₁
Molecular Weight:809.926
Hs Code.:

Synonyms:trideuteriomethyl O-(3,4-di-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-mannopyranoside

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Chemical Property of trideuteriomethyl O-(3,4-di-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-mannopyranoside

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Technology Process of trideuteriomethyl O-(3,4-di-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-mannopyranoside

There total 7 articles about trideuteriomethyl O-(3,4-di-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 100638-55-9
trideuteriomethyl 2,3,4-tri-O-benzyl-6-O-(2,6-di-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranosyl)-β-D-mannopyranoside

: 105608-14-8
trideuteriomethyl O-(3,4-di-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-mannopyranoside

Guidance literature:: With sodium methylate; In methanol; for 1h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90207-6

Reference yield:

: 65827-57-8
1,2,6-tri-O-acetyl-3,4-di-O-benzyl-α-D-mannopyranose

: 105608-14-8
trideuteriomethyl O-(3,4-di-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: HBr / CH₂Cl₂ / 3 h / 0 °C

2: thallium zeolite / CH₂Cl₂ / 92 h / Ambient temperature; comparison of various promoters on anomer rates

3: 94 percent / sodium methoxide / methanol / 1 h / Ambient temperature

With thallium zeolite; hydrogen bromide; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)90207-6

Reference yield:

: 65556-30-1
1,6-di-O-acetyl-2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 105608-14-8
trideuteriomethyl O-(3,4-di-O-benzyl-α-D-mannopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: HBr / CH₂Cl₂ / 2 h / 0 °C

2: Ag zeolite / CH₂Cl₂ / 2 h

3: 75 percent / sodium methoxide / methanol / 2 h / Ambient temperature

4: thallium zeolite / CH₂Cl₂ / 92 h / Ambient temperature; comparison of various promoters on anomer rates

5: 94 percent / sodium methoxide / methanol / 1 h / Ambient temperature

With Ag Zeolite; thallium zeolite; hydrogen bromide; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)90207-6