1-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol

Base Information

Chemical Name:1-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol
CAS No.:161664-57-9
Molecular Formula:C₃₄H₄₈O₆Si
Molecular Weight:580.837
Hs Code.:

Synonyms:1-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol

Suppliers and Price of 1-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol

There total 3 articles about 1-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 151838-13-0
2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol

: 161664-57-9
1-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol

Guidance literature:: With 1H-imidazole; In dichloromethane;

Reference yield:

: 20227-17-2,20227-12-7,20227-24-1,36725-73-2
2,3,4-tri-O-methyl-D-galacitol

: 161664-57-9
1-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / DMAP, pyridine / 24 h / Ambient temperature

2: 77 percent / imidazole / CH₂Cl₂

With pyridine; 1H-imidazole; dmap; In dichloromethane;

Reference yield:

: 4060-09-7,4060-13-3,4239-83-2,5856-24-6,7330-01-0,40896-77-3,58894-01-2
2.3.4-Tri-O-methyl-D-galactose

: 161664-57-9
1-O-(tert-butyldimethylsilyl)-2,3,4-tri-O-methyl-6-O-trutyl-D-galacitol

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaBH₄ / ethanol

2: 37 percent / DMAP, pyridine / 24 h / Ambient temperature

3: 77 percent / imidazole / CH₂Cl₂

With pyridine; 1H-imidazole; dmap; sodium tetrahydroborate; In ethanol; dichloromethane;