tert-butyl N-(2-methoxyphenyl)carbamate

Base Information

Chemical Name:tert-butyl N-(2-methoxyphenyl)carbamate
CAS No.:154150-18-2
Molecular Formula:C12H17 N O3
Molecular Weight:223.272
Hs Code.:2924297099
European Community (EC) Number:939-170-4,803-043-0
DSSTox Substance ID:DTXSID90406855
Nikkaji Number:J764.768I
Wikidata:Q82211974
Mol file:154150-18-2.mol

Synonyms:154150-18-2;tert-butyl N-(2-methoxyphenyl)carbamate;tert-Butyl (2-methoxyphenyl)carbamate;Tert-butyl 2-methoxyphenylcarbamate;N-BOC-2-METHOXYANILINE;MFCD07127728;(2-METHOXYPHENYL)-CARBAMIC ACID, 1,1-DIMETHYL ETHYL ESTER;tert-Butyl(2-methoxyphenyl)carbamate;SCHEMBL729221;N-Boc-2-methoxyaniline, 97%;DTXSID90406855;DHSWMVURURVRDB-UHFFFAOYSA-N;2-Methoxyaniline, N-BOC protected;(2-MEHTOXYPHENYL)-CARBAMIC ACID 1,1-DIMETHYL ETHYL ESTER;AKOS003581112;N-(t-butoxycarbonyl)-2-methoxyaniline;AB30560;SS-4421;tert-butyl-N-(2-methoxyphenyl)carbamate;AC-14184;SY158196;CS-0154411;FT-0740770;EN300-160612;F14355;A849986;J-500830;Z1258794272

Suppliers and Price of tert-butyl N-(2-methoxyphenyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
tert-ButylN-(2-Methoxyphenyl)carbamate
500mg
$ 155.00

SynQuest Laboratories
2-Methoxyaniline, N-Boc protected
1 g
$ 122.00

SynQuest Laboratories
2-Methoxyaniline, N-Boc protected
500 mg
$ 96.00

Sigma-Aldrich
N-Boc-2-methoxyaniline 97%
5g
$ 76.00

Matrix Scientific
tert-Butyl N-(2-methoxyphenyl)carbamate >97%
1g
$ 159.00

Matrix Scientific
tert-Butyl N-(2-methoxyphenyl)carbamate >97%
500mg
$ 126.00

Crysdot
tert-Butyl(2-methoxyphenyl)carbamate 95+%
5g
$ 322.00

American Custom Chemicals Corporation
(2-METHOXYPHENYL)-CARBAMIC ACID, 1,1-DIMETHYL ETHYL ESTER 95.00%
1G
$ 945.95

AK Scientific
tert-ButylN-(2-methoxyphenyl)carbamate
1g
$ 264.00

Acrotein
N-Boc-2-methoxyaniline 97%
25g
$ 385.00

Total 24 raw suppliers

Chemical Property of tert-butyl N-(2-methoxyphenyl)carbamate

Chemical Property:

Vapor Pressure:0.00492mmHg at 25°C
Melting Point:33.5-35.0°C
Boiling Point:276°Cat760mmHg
Flash Point:120.7°C
PSA：47.56000
Density:1.102g/cm³
LogP:3.11520
Storage Temp.:Sealed in dry,Room Temperature
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:223.12084340
Heavy Atom Count:16
Complexity:235

Purity/Quality:

99%, ^*data from raw suppliers

tert-ButylN-(2-Methoxyphenyl)carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn
Statements: 22-36/37/38
Safety Statements: 26

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NC1=CC=CC=C1OC

Technology Process of tert-butyl N-(2-methoxyphenyl)carbamate

There total 8 articles about tert-butyl N-(2-methoxyphenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 90-04-0
2-methoxy-phenylamine

: 154150-18-2
tert-butyl 2-methoxyphenylcarbamate

Guidance literature:: In tetrahydrofuran; Heating;
DOI:10.1002/anie.200604038

Reference yield: 99.0%

: 4248-19-5
tert-butyl carbazate

: 766-51-8
2-Chloroanisole

: 154150-18-2
tert-butyl 2-methoxyphenylcarbamate

Guidance literature:: With 4-diphenylphosphino-13-dicyclohexylphosphino-[2.2]paracyclophane; water; palladium diacetate; caesium carbonate; In 1,4-dioxane; at 125 ℃; for 24h;
DOI:10.1039/c1cc14844c

Reference yield: 93.0%

: 4248-19-5
tert-butyl carbazate

: 578-57-4
2-bromoanisole

: 154150-18-2
tert-butyl 2-methoxyphenylcarbamate

Guidance literature:: With ?di-tert-butyl(2,2-diphenyl-1-methyl-1-cyclopropyl)phosphine; bis(η3-allyl-μ-chloropalladium(II)); sodium t-butanolate; In water; at 50 ℃; for 24h; Inert atmosphere; Green chemistry;
DOI:10.1039/c3gc42188k