Technology Process of C23H36N2O
There total 4 articles about C23H36N2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C23H34N2;
With
sulfuric acid;
for 18h;
Inert atmosphere;
Heating;
With
ammonium hydroxide;
In
water; ethyl acetate;
at 0 ℃;
Inert atmosphere;
DOI:10.1016/j.tet.2011.02.027
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: hydrogenchloride / methanol; water / 124 h / 20 °C / Inert atmosphere
3.1: sulfuric acid / 18 h / Inert atmosphere; Heating
3.2: 0 °C / Inert atmosphere
With
hydrogenchloride; oxalyl dichloride; sulfuric acid; dimethyl sulfoxide;
In
methanol; dichloromethane; water;
DOI:10.1016/j.tet.2011.02.027
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogenchloride / methanol; water / 124 h / 20 °C / Inert atmosphere
2.1: sulfuric acid / 18 h / Inert atmosphere; Heating
2.2: 0 °C / Inert atmosphere
With
hydrogenchloride; sulfuric acid;
In
methanol; water;
DOI:10.1016/j.tet.2011.02.027