N₂-isobutyryl-5'-O-(tert-butyldimethylsilyl)-3'-O-(4,4'-dimethoxytrityl)-2'-deoxyguanosine

Base Information

• Chemical Name: N₂-isobutyryl-5'-O-(tert-butyldimethylsilyl)-3'-O-(4,4'-dimethoxytrityl)-2'-deoxyguanosine
• CAS No.: 213882-93-0
• Molecular Formula: C₄₁H₅₁N₅O₇Si
• Molecular Weight: 753.971

Synonyms:N₂-isobutyryl-5'-O-(tert-butyldimethylsilyl)-3'-O-(4,4'-dimethoxytrityl)-2'-deoxyguanosine

Chemical Property of N₂-isobutyryl-5'-O-(tert-butyldimethylsilyl)-3'-O-(4,4'-dimethoxytrityl)-2'-deoxyguanosine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N₂-isobutyryl-5'-O-(tert-butyldimethylsilyl)-3'-O-(4,4'-dimethoxytrityl)-2'-deoxyguanosine

There total 3 articles about N₂-isobutyryl-5'-O-(tert-butyldimethylsilyl)-3'-O-(4,4'-dimethoxytrityl)-2'-deoxyguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

4,4'-dimethoxytrityl chloride (40615-36-9) + N2-isobutyryl-5′-O-(tert-butyldimethylsilyl)-2′-deoxyguanosine (85326-10-9) → N2-isobutyryl-5'-O-(tert-butyldimethylsilyl)-3'-O-(4,4'-dimethoxytrityl)-2'-deoxyguanosine (213882-93-0)

Guidance literature:

With pyridine; at 40 ℃;

Reference yield:

N-isobutyryl-2'-deoxyguanosine (68892-42-2) → N2-isobutyryl-5'-O-(tert-butyldimethylsilyl)-3'-O-(4,4'-dimethoxytrityl)-2'-deoxyguanosine (213882-93-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 20 °C

2: pyridine / 20 °C

With pyridine;

DOI:10.1080/07328319808004703

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) → N2-isobutyryl-5'-O-(tert-butyldimethylsilyl)-3'-O-(4,4'-dimethoxytrityl)-2'-deoxyguanosine (213882-93-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 20 °C

2: pyridine / 20 °C

With pyridine;

DOI:10.1080/07328319808004703

upstream raw materials:

4,4'-dimethoxytrityl chloride

N²-isobutyryl-5′-O-(tert-butyldimethylsilyl)-2′-deoxyguanosine

N-isobutyryl-2'-deoxyguanosine

tert-butyldimethylsilyl chloride

Downstream raw materials:

3'-O-dimethoxytrityl-N²-isobutyryl-2'-deoxyguanosine

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