2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-3-deoxy-1-diphenyl phosphate

Base Information

Chemical Name:2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-3-deoxy-1-diphenyl phosphate
CAS No.:899827-38-4
Molecular Formula:C₄₅H₅₃O₈PSi
Molecular Weight:780.97
Hs Code.:

Synonyms:2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-3-deoxy-1-diphenyl phosphate

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Chemical Property of 2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-3-deoxy-1-diphenyl phosphate

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Technology Process of 2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-3-deoxy-1-diphenyl phosphate

There total 3 articles about 2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-3-deoxy-1-diphenyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 899827-37-3
2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester

: 899827-38-4
2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-3-deoxy-1-diphenyl phosphate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 4h; Heating;
DOI:10.1021/jo060702s

Reference yield:

: 376590-85-1
1-O-diphenylphosphate-2,4,6-tri-O-benzyl-D-myo-inositol

: 899827-38-4
2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-3-deoxy-1-diphenyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / DMAP; pyridine / CH₂Cl₂

2: 90 percent / 2,6-lutidine / CH₂Cl₂ / 3 h

3: 70 percent / Bu₃SnH; AIBN / toluene / 4 h / Heating

With pyridine; 2,6-dimethylpyridine; dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In dichloromethane; toluene;
DOI:10.1021/jo060702s

Reference yield:

: 816426-16-1
2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester

: 899827-38-4
2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-3-deoxy-1-diphenyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / 2,6-lutidine / CH₂Cl₂ / 3 h

2: 70 percent / Bu₃SnH; AIBN / toluene / 4 h / Heating

With 2,6-dimethylpyridine; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In dichloromethane; toluene;
DOI:10.1021/jo060702s