2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester

Base Information

• Chemical Name: 2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester
• CAS No.: 816426-16-1
• Molecular Formula: C₄₆H₄₃O₁₀PS
• Molecular Weight: 818.881

Synonyms:2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester

Chemical Property of 2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester

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Technology Process of 2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester

There total 1 articles about 2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

phenylcarbonochloridothioate (1005-56-7) + 1-O-diphenylphosphate-2,4,6-tri-O-benzyl-D-myo-inositol (376590-85-1) → 2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester (816426-16-1)

Guidance literature:

With pyridine; dmap; In dichloromethane; for 2.5h;

DOI:10.1021/ja047360x

Reference yield: 91.0%

acetic anhydride (108-24-7) + 2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester (816426-16-1) → 5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester (816426-22-9)

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 4h;

DOI:10.1021/ja047360x

Reference yield: 90.0%

t-butyldimethylsiyl triflate (69739-34-0) + 2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester (816426-16-1) → 2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester (899827-37-3)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; for 3h;

DOI:10.1021/jo060702s

upstream raw materials:

phenylcarbonochloridothioate

1-O-diphenylphosphate-2,4,6-tri-O-benzyl-D-myo-inositol

Downstream raw materials:

5-O-acetate-2,4,6-tri-O-benzyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester

2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-3-O-thiocarbonic acid phenyl ester

2,4,6-tri-O-benzyl-D-myo-inositol-3-deoxy-1-dibenzyl phosphate

2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-3-deoxy-1-diphenyl phosphate

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