2,5-bis(hexyloxy)-N'1,N'4-bis(3-(4-nitrophenoxy)benzoyl)terephthalohydrazide

Base Information

Chemical Name:2,5-bis(hexyloxy)-N'1,N'4-bis(3-(4-nitrophenoxy)benzoyl)terephthalohydrazide
CAS No.:1253119-92-4
Molecular Formula:C₄₆H₄₈N₆O₁₂
Molecular Weight:876.92
Hs Code.:

Synonyms:2,5-bis(hexyloxy)-N'1,N'4-bis(3-(4-nitrophenoxy)benzoyl)terephthalohydrazide

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Chemical Property of 2,5-bis(hexyloxy)-N'1,N'4-bis(3-(4-nitrophenoxy)benzoyl)terephthalohydrazide

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Technology Process of 2,5-bis(hexyloxy)-N'1,N'4-bis(3-(4-nitrophenoxy)benzoyl)terephthalohydrazide

There total 9 articles about 2,5-bis(hexyloxy)-N'1,N'4-bis(3-(4-nitrophenoxy)benzoyl)terephthalohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3-(4-nitro-phenoxy)-benzoic acid hydrazide

: 103761-95-1
2,5-bis(hexyloxy)terephthaloxy chrloride

: 1253119-92-4
2,5-bis(hexyloxy)-N'1,N'4-bis(3-(4-nitrophenoxy)benzoyl)terephthalohydrazide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 12h;

Reference yield:

: 111-25-1
1-bromo-hexane

: 1253119-92-4
2,5-bis(hexyloxy)-N'1,N'4-bis(3-(4-nitrophenoxy)benzoyl)terephthalohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 95 °C

2.1: potassium hydroxide / ethanol / 12 h / Reflux

2.2: pH 4

3.1: N,N-dimethyl-formamide; thionyl chloride / 6 h / 80 °C

4.1: tetrahydrofuran / 12 h / 20 °C

With thionyl chloride; potassium carbonate; N,N-dimethyl-formamide; potassium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1253119-92-4
2,5-bis(hexyloxy)-N'1,N'4-bis(3-(4-nitrophenoxy)benzoyl)terephthalohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / dimethyl sulfoxide / 12 h / 130 °C

2: hydrogenchloride / water / 12 h / 110 °C

3: hydrazine hydrate / ethanol / 24 h / Reflux

4: tetrahydrofuran / 12 h / 20 °C

With hydrogenchloride; potassium carbonate; hydrazine hydrate; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide;