Technology Process of C32H31NO9
There total 4 articles about C32H31NO9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C40H39NO13;
With
sodium methylate;
In
methanol;
at 20 ℃;
for 12h;
In
methanol;
pH=5;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: silver(l) oxide / acetonitrile / 12 h / 20 °C / Darkness; Inert atmosphere
2.1: sodium tetrahydroborate / isopropyl alcohol; chloroform / 12 h / 0 - 20 °C / Inert atmosphere
3.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C
4.1: sodium methylate / methanol / 12 h / 20 °C
4.2: Dowex.(R). H+ resin / pH 5
With
dmap; sodium tetrahydroborate; sodium methylate; triethylamine; silver(l) oxide;
In
methanol; dichloromethane; chloroform; isopropyl alcohol; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: silver(l) oxide / acetonitrile / 12 h / 20 °C / Darkness; Inert atmosphere
2.1: sodium tetrahydroborate / isopropyl alcohol; chloroform / 12 h / 0 - 20 °C / Inert atmosphere
3.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C
4.1: sodium methylate / methanol / 12 h / 20 °C
4.2: Dowex.(R). H+ resin / pH 5
With
dmap; sodium tetrahydroborate; sodium methylate; triethylamine; silver(l) oxide;
In
methanol; dichloromethane; chloroform; isopropyl alcohol; acetonitrile;