2-hydroxy-3-nitro-4-phenyl-butanal diethyl acetal

Base Information

• Chemical Name: 2-hydroxy-3-nitro-4-phenyl-butanal diethyl acetal
• CAS No.: 132499-01-5
• Molecular Formula: C₁₄H₂₁NO₅
• Molecular Weight: 283.324
• Mol file: 132499-01-5.mol

Synonyms:2-hydroxy-3-nitro-4-phenyl-butanal diethyl acetal

Chemical Property of 2-hydroxy-3-nitro-4-phenyl-butanal diethyl acetal

Chemical Property:

Purity/Quality:

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Technology Process of 2-hydroxy-3-nitro-4-phenyl-butanal diethyl acetal

There total 1 articles about 2-hydroxy-3-nitro-4-phenyl-butanal diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

diethoxyacetaldehyde (5344-23-0) + 2-Phenylnitroethane (6125-24-2) → 2-hydroxy-3-nitro-4-phenyl-butanal diethyl acetal (132499-01-5)

Guidance literature:

With potassium carbonate; at 50 ℃; for 6h;

DOI:10.1016/0968-0896(96)00115-0

Reference yield: 93.0%

2-hydroxy-3-nitro-4-phenyl-butanal diethyl acetal (132499-01-5) → 3-amino-2-hydroxy-4-phenyl-butanal diethyl acetal (132499-03-7)

Guidance literature:

With hydrogen; nickel; under 760 Torr; Ambient temperature;

DOI:10.1016/0968-0896(96)00115-0

upstream raw materials:

diethoxyacetaldehyde

2-Phenylnitroethane

Downstream raw materials:

3-amino-2-hydroxy-4-phenyl-butanal diethyl acetal