N-(dec-1-yn-3-yl) p-tolylsulfonamide

Base Information

Chemical Name:N-(dec-1-yn-3-yl) p-tolylsulfonamide
CAS No.:57981-24-5
Molecular Formula:C₁₇H₂₅NO₂S
Molecular Weight:307.457
Hs Code.:

Synonyms:N-(dec-1-yn-3-yl) p-tolylsulfonamide

Suppliers and Price of N-(dec-1-yn-3-yl) p-tolylsulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of N-(dec-1-yn-3-yl) p-tolylsulfonamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of N-(dec-1-yn-3-yl) p-tolylsulfonamide

There total 1 articles about N-(dec-1-yn-3-yl) p-tolylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 764-93-2
1-decyne

: 851-06-9
bis(p-toluenesulfonyl) sulfur diimide

: 57981-24-5
N-(dec-1-yn-3-yl) p-tolylsulfonamide

Guidance literature:: Multistep reaction; (i) CH₂Cl₂, (ii) aq. K₂CO₃, MeOH;
DOI:10.1021/jo00863a051

Reference yield: 59.0%

: 57981-24-5
N-(dec-1-yn-3-yl) p-tolylsulfonamide

: 100-52-7
benzaldehyde

: 1208114-91-3
N-(1-phenylundeca-1,2-dien-4-yl) p-tolylsulfonamide

Guidance literature:: With morpholine; zinc(II) iodide; In toluene; at 130 ℃; for 6.4h; Inert atmosphere; Sealed tube;
DOI:10.1021/ja910503k

Reference yield: 35.0%

: 57981-24-5
N-(dec-1-yn-3-yl) p-tolylsulfonamide

: 123-72-8
butyraldehyde

: 1314716-05-6
C₂₁H₃₃NO₂S

Guidance literature:: With copper(l) iodide; N-cyclohexyl-cyclohexanamine; In toluene; at 200 ℃; for 1h; Microwave irradiation;
DOI:10.1055/s-0030-1259936