O₂-(2,4-dinitrophenyl)-1-[4-(tert-butoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate

Base Information

• Chemical Name: O₂-(2,4-dinitrophenyl)-1-[4-(tert-butoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate
• CAS No.: 903568-75-2
• Molecular Formula: C₁₅H₂₀N₆O₈
• Molecular Weight: 412.359

Synonyms:O₂-(2,4-dinitrophenyl)-1-[4-(tert-butoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate

Chemical Property of O₂-(2,4-dinitrophenyl)-1-[4-(tert-butoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of O₂-(2,4-dinitrophenyl)-1-[4-(tert-butoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate

There total 3 articles about O₂-(2,4-dinitrophenyl)-1-[4-(tert-butoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

sodium 1-[4-(tert-butoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → O2-(2,4-dinitrophenyl)-1-[4-(tert-butoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate (903568-75-2)

Guidance literature:

With sodium hydrogencarbonate; In tert-butyl alcohol; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

sodium 1-[4-(tert-butoxycarbonyl)piperazin-1-yl]diazen-1-ium-1,2-diolate + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → C15H20N6(1+)O8(1-) (903568-75-2)

Guidance literature:

With sodium hydrogencarbonate; In tert-butyl alcohol; at 20 ℃; for 24h;

DOI:10.1021/jm060022h

Reference yield:

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) + 1-t-Butoxycarbonylpiperazine (57260-71-6) → C15H20N6(1+)O8(1-) (903568-75-2)

Guidance literature:

1-t-Butoxycarbonylpiperazine; With nitrogen(II) oxide; sodium methylate; In methanol; diethyl ether; under 2280.15 Torr;

2,4-Dinitrofluorobenzene; With sodium hydrogencarbonate; In tert-butyl alcohol; Further stages.;

DOI:10.1016/j.bmcl.2007.12.044

upstream raw materials:

2,4-Dinitrofluorobenzene

1-t-Butoxycarbonylpiperazine

Downstream raw materials:

C₁₀H₁₂N₆O₆*ClH

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