5-Oxo-2,7-di-p-tolyl-1,4,6-triaza-tricyclo[5.1.0.0^2,4]octane-6-sulfonyl chloride

Base Information

• Chemical Name: 5-Oxo-2,7-di-p-tolyl-1,4,6-triaza-tricyclo[5.1.0.0^2,4]octane-6-sulfonyl chloride
• CAS No.: 136611-97-7
• Molecular Formula: C₁₉H₁₈ClN₃O₃S
• Molecular Weight: 403.889

Synonyms:5-Oxo-2,7-di-p-tolyl-1,4,6-triaza-tricyclo[5.1.0.0^2,4]octane-6-sulfonyl chloride

Chemical Property of 5-Oxo-2,7-di-p-tolyl-1,4,6-triaza-tricyclo[5.1.0.0^2,4]octane-6-sulfonyl chloride

Chemical Property:

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Technology Process of 5-Oxo-2,7-di-p-tolyl-1,4,6-triaza-tricyclo[5.1.0.0^2,4]octane-6-sulfonyl chloride

There total 2 articles about 5-Oxo-2,7-di-p-tolyl-1,4,6-triaza-tricyclo[5.1.0.0^2,4]octane-6-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.8%

isocyanate de chlorosulfonyle (1189-71-5) + 3-p-tolyl-2H-azirine (32687-33-5) → 2,5-di-(4-methylphenyl)pyrazine (16873-56-6) + C19H18ClN3O3S (136612-00-5) + 5-Oxo-2,7-di-p-tolyl-1,4,6-triaza-tricyclo[5.1.0.02,4]octane-6-sulfonyl chloride (136611-97-7)

Guidance literature:

In dichloromethane; at -78 ℃; for 0.5h;

DOI:10.1080/00397919108021065

Reference yield:

isocyanate de chlorosulfonyle (1189-71-5) + 3-p-tolyl-2H-azirine (32687-33-5) → C19H18ClN3O3S (136612-00-5) + 5-Oxo-2,7-di-p-tolyl-1,4,6-triaza-tricyclo[5.1.0.02,4]octane-6-sulfonyl chloride (136611-97-7)

Guidance literature:

at -78 ℃;

DOI:10.1080/00397919308018610

Reference yield: 96.0%

5-Oxo-2,7-di-p-tolyl-1,4,6-triaza-tricyclo[5.1.0.02,4]octane-6-sulfonyl chloride (136611-97-7) → (4Z,7Z)-4,7-Di-p-tolyl-3,6-dihydro-1H-[1,3,6]triazocin-2-one

Guidance literature:

With potassium hydroxide; In acetone;

DOI:10.1080/00397919308018610

upstream raw materials:

isocyanate de chlorosulfonyle

3-p-tolyl-2H-azirine

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