(R)-Methoxy-phenyl-acetic acid 2-{(1R,2R)-2-[2-((R)-2-methoxy-2-phenyl-acetoxy)-phenyl]-cyclopentyl}-phenyl ester

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Chemical Name:(R)-Methoxy-phenyl-acetic acid 2-{(1R,2R)-2-[2-((R)-2-methoxy-2-phenyl-acetoxy)-phenyl]-cyclopentyl}-phenyl ester
CAS No.:190248-08-9
Molecular Formula:C₃₅H₃₄O₆
Molecular Weight:550.651
Hs Code.:

Synonyms:(R)-Methoxy-phenyl-acetic acid 2-{(1R,2R)-2-[2-((R)-2-methoxy-2-phenyl-acetoxy)-phenyl]-cyclopentyl}-phenyl ester

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Chemical Property of (R)-Methoxy-phenyl-acetic acid 2-{(1R,2R)-2-[2-((R)-2-methoxy-2-phenyl-acetoxy)-phenyl]-cyclopentyl}-phenyl ester

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Technology Process of (R)-Methoxy-phenyl-acetic acid 2-{(1R,2R)-2-[2-((R)-2-methoxy-2-phenyl-acetoxy)-phenyl]-cyclopentyl}-phenyl ester

There total 7 articles about (R)-Methoxy-phenyl-acetic acid 2-{(1R,2R)-2-[2-((R)-2-methoxy-2-phenyl-acetoxy)-phenyl]-cyclopentyl}-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4945-79-3
1,5-bis(2-hydroxyphenyl)-1,5-pentanedione

: 190248-08-9
(R)-Methoxy-phenyl-acetic acid 2-{(1R,2R)-2-[2-((R)-2-methoxy-2-phenyl-acetoxy)-phenyl]-cyclopentyl}-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / KOH / ethanol

2: 57 percent / TiCl₄/Zn / tetrahydrofuran / 22 h / Ambient temperature

3: 86 percent / Et₃SiH/CF₃CO₂H / CH₂Cl₂ / 24 h / Ambient temperature

4: 84 percent / KOtBu / dimethylsulfoxide / 6 h / 100 °C

5: 95 percent / PBr₃ / CH₂Cl₂ / 5.5 h / 0 - 20 °C

6: DCC, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

With triethylsilane; dmap; potassium hydroxide; potassium tert-butylate; phosphorus tribromide; titanium tetrachloride; dicyclohexyl-carbodiimide; trifluoroacetic acid; zinc; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(97)00421-8

Reference yield:

: 63359-17-1
1.2-Di-(2'-methoxyphenyl)-Δ¹-cyclopenten

: 190248-08-9
(R)-Methoxy-phenyl-acetic acid 2-{(1R,2R)-2-[2-((R)-2-methoxy-2-phenyl-acetoxy)-phenyl]-cyclopentyl}-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / Et₃SiH/CF₃CO₂H / CH₂Cl₂ / 24 h / Ambient temperature

2: 84 percent / KOtBu / dimethylsulfoxide / 6 h / 100 °C

3: 95 percent / PBr₃ / CH₂Cl₂ / 5.5 h / 0 - 20 °C

4: DCC, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

With triethylsilane; dmap; potassium tert-butylate; phosphorus tribromide; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(97)00421-8

Reference yield:

: 66-76-2
dicoumarol

: 190248-08-9
(R)-Methoxy-phenyl-acetic acid 2-{(1R,2R)-2-[2-((R)-2-methoxy-2-phenyl-acetoxy)-phenyl]-cyclopentyl}-phenyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 99 percent / 10percent KOH (aq.) / H₂O / 12 h / Heating

2: 87 percent / KOH / ethanol

3: 57 percent / TiCl₄/Zn / tetrahydrofuran / 22 h / Ambient temperature

4: 86 percent / Et₃SiH/CF₃CO₂H / CH₂Cl₂ / 24 h / Ambient temperature

5: 84 percent / KOtBu / dimethylsulfoxide / 6 h / 100 °C

6: 95 percent / PBr₃ / CH₂Cl₂ / 5.5 h / 0 - 20 °C

7: DCC, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

With triethylsilane; dmap; potassium hydroxide; potassium tert-butylate; phosphorus tribromide; titanium tetrachloride; dicyclohexyl-carbodiimide; trifluoroacetic acid; zinc; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(97)00421-8