N-(4-{[3-methyl-4-(2-chloroacetylamino)phenyl]methyl}-2-(tributylstannyl)phenyl)-2-chloroacetamide

Base Information

Chemical Name:N-(4-{[3-methyl-4-(2-chloroacetylamino)phenyl]methyl}-2-(tributylstannyl)phenyl)-2-chloroacetamide
CAS No.:1279721-75-3
Molecular Formula:C₃₀H₄₄Cl₂N₂O₂Sn
Molecular Weight:654.308
Hs Code.:

Synonyms:N-(4-{[3-methyl-4-(2-chloroacetylamino)phenyl]methyl}-2-(tributylstannyl)phenyl)-2-chloroacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-{[3-methyl-4-(2-chloroacetylamino)phenyl]methyl}-2-(tributylstannyl)phenyl)-2-chloroacetamide

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Technology Process of N-(4-{[3-methyl-4-(2-chloroacetylamino)phenyl]methyl}-2-(tributylstannyl)phenyl)-2-chloroacetamide

There total 4 articles about N-(4-{[3-methyl-4-(2-chloroacetylamino)phenyl]methyl}-2-(tributylstannyl)phenyl)-2-chloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1279721-74-2
4,4'-diamino-3-methyl-3'-(tributylstannyl)diphenylmethane

: 79-04-9
chloroacetyl chloride

: 1279721-75-3
N-(4-{[3-methyl-4-(2-chloroacetylamino)phenyl]methyl}-2-(tributylstannyl)phenyl)-2-chloroacetamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1002/cmdc.201300167

Reference yield:

: 95-53-4
o-toluidine

: 1279721-75-3
N-(4-{[3-methyl-4-(2-chloroacetylamino)phenyl]methyl}-2-(tributylstannyl)phenyl)-2-chloroacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 18 h / 25 °C / Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / 25 - 100 °C

3: triethylamine / dichloromethane / 0.17 h / 0 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In methanol; dichloromethane; toluene;
DOI:10.1002/cmdc.201300167

Reference yield:

: 1279721-72-0
4,4'-diamino-3-iodo-3'-methyldiphenylmethane

: 1279721-75-3
N-(4-{[3-methyl-4-(2-chloroacetylamino)phenyl]methyl}-2-(tributylstannyl)phenyl)-2-chloroacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / 25 - 100 °C

2: triethylamine / dichloromethane / 0.17 h / 0 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In dichloromethane; toluene;
DOI:10.1002/cmdc.201300167