(S)-2-[3-(Acetyl-methyl-amino)-2-diazo-3-oxo-propionyloxy]-3-methyl-butyric acid benzyl ester

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Chemical Name:(S)-2-[3-(Acetyl-methyl-amino)-2-diazo-3-oxo-propionyloxy]-3-methyl-butyric acid benzyl ester
CAS No.:431069-73-7
Molecular Formula:C₁₈H₂₁N₃O₆
Molecular Weight:375.381
Hs Code.:

Synonyms:(S)-2-[3-(Acetyl-methyl-amino)-2-diazo-3-oxo-propionyloxy]-3-methyl-butyric acid benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-[3-(Acetyl-methyl-amino)-2-diazo-3-oxo-propionyloxy]-3-methyl-butyric acid benzyl ester

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Technology Process of (S)-2-[3-(Acetyl-methyl-amino)-2-diazo-3-oxo-propionyloxy]-3-methyl-butyric acid benzyl ester

There total 1 articles about (S)-2-[3-(Acetyl-methyl-amino)-2-diazo-3-oxo-propionyloxy]-3-methyl-butyric acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 65138-05-8
(S)-2-hydroxy-3-methylbutyric acid benzyl ester

: 431069-31-7
3-(acetyl-methyl-amino)-3-oxo-propionic acid

: 431069-73-7
(S)-2-[3-(Acetyl-methyl-amino)-2-diazo-3-oxo-propionyloxy]-3-methyl-butyric acid benzyl ester

Guidance literature:: (S)-2-hydroxy-3-methylbutyric acid benzyl ester; 3-(acetyl-methyl-amino)-3-oxo-propionic acid; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 5h;

With triethylamine; Methanesulfonyl azide; In diethyl ether; at 20 ℃; for 5h; Further stages.;
DOI:10.1021/ol017263y