4'-methoxy-1,3-dimethyl-7'-(1,3-dimethyl-2,4,6-trioxoperhydropyrimidin-5-yl)-2,4,6-trioxospiro[perhydropyrimidine-5,6'-(5',6',7',8'-tetrahydro[1,3]dioxolo[4,5-g]naphthalene)]

Base Information

• Chemical Name: 4'-methoxy-1,3-dimethyl-7'-(1,3-dimethyl-2,4,6-trioxoperhydropyrimidin-5-yl)-2,4,6-trioxospiro[perhydropyrimidine-5,6'-(5',6',7',8'-tetrahydro[1,3]dioxolo[4,5-g]naphthalene)]
• CAS No.: 471248-47-2
• Molecular Formula: C₂₃H₂₄N₄O₉
• Molecular Weight: 500.465

Synonyms:4'-methoxy-1,3-dimethyl-7'-(1,3-dimethyl-2,4,6-trioxoperhydropyrimidin-5-yl)-2,4,6-trioxospiro[perhydropyrimidine-5,6'-(5',6',7',8'-tetrahydro[1,3]dioxolo[4,5-g]naphthalene)]

Chemical Property of 4'-methoxy-1,3-dimethyl-7'-(1,3-dimethyl-2,4,6-trioxoperhydropyrimidin-5-yl)-2,4,6-trioxospiro[perhydropyrimidine-5,6'-(5',6',7',8'-tetrahydro[1,3]dioxolo[4,5-g]naphthalene)]

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Technology Process of 4'-methoxy-1,3-dimethyl-7'-(1,3-dimethyl-2,4,6-trioxoperhydropyrimidin-5-yl)-2,4,6-trioxospiro[perhydropyrimidine-5,6'-(5',6',7',8'-tetrahydro[1,3]dioxolo[4,5-g]naphthalene)]

There total 4 articles about 4'-methoxy-1,3-dimethyl-7'-(1,3-dimethyl-2,4,6-trioxoperhydropyrimidin-5-yl)-2,4,6-trioxospiro[perhydropyrimidine-5,6'-(5',6',7',8'-tetrahydro[1,3]dioxolo[4,5-g]naphthalene)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

1,3-dimethylbarbituric acid (769-42-6) + 5-(4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo[4,5-g]isoquinolin-5-yl)-1,3-dimethylbarbituric acid (464171-44-6) → 1,3,5-trimethylbarbituric acid (7358-61-4) + hydrocotarnine (550-10-7) + 4'-methoxy-1,3-dimethyl-7'-(1,3-dimethyl-2,4,6-trioxoperhydropyrimidin-5-yl)-2,4,6-trioxospiro[perhydropyrimidine-5,6'-(5',6',7',8'-tetrahydro[1,3]dioxolo[4,5-g]naphthalene)] (471248-47-2)

Guidance literature:

With ISOPROPYLAMIDE; triethylamine; at 160 ℃; for 0.333333h;

DOI:10.1023/A:1020983527851

Reference yield: 44.0%

1,3-dimethylbarbituric acid (769-42-6) + 4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo[4,5-g]isoquinolin-5-ol (82-54-2) → 1,3,5-trimethylbarbituric acid (7358-61-4) + hydrocotarnine (550-10-7) + 4'-methoxy-1,3-dimethyl-7'-(1,3-dimethyl-2,4,6-trioxoperhydropyrimidin-5-yl)-2,4,6-trioxospiro[perhydropyrimidine-5,6'-(5',6',7',8'-tetrahydro[1,3]dioxolo[4,5-g]naphthalene)] (471248-47-2)

Guidance literature:

With ISOPROPYLAMIDE; triethylamine; at 160 ℃; for 0.333333h;

DOI:10.1023/A:1020983527851

Reference yield: 35.0%

1,3-dimethylbarbituric acid (769-42-6) + (4-methoxy-6-methyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinolin-5-yl)-phenyl-acetonitrile → 1,3,5-trimethylbarbituric acid (7358-61-4) + hydrocotarnine (550-10-7) + 4'-methoxy-1,3-dimethyl-7'-(1,3-dimethyl-2,4,6-trioxoperhydropyrimidin-5-yl)-2,4,6-trioxospiro[perhydropyrimidine-5,6'-(5',6',7',8'-tetrahydro[1,3]dioxolo[4,5-g]naphthalene)] (471248-47-2)

Guidance literature:

With ISOPROPYLAMIDE; triethylamine; at 160 ℃; for 0.333333h;

DOI:10.1023/A:1020983527851

upstream raw materials:

1,3-dimethylbarbituric acid

4-methoxy-6-methyl-5-nitromethyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline

5-(4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo[4,5-g]isoquinolin-5-yl)-1,3-dimethylbarbituric acid

4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo[4,5-g]isoquinolin-5-ol

Downstream raw materials:

1,3-dimethyl-2,4,6-trioxoperhydropyrimidine-5-spiro-6'-{4'-methoxy-7'-(1,3-dimethyl-5-[2-(4-pyridyl)ethyl]-2,4,6-trioxoperhydropyrimidin-5-yl)-5',6',7',8'-tetrahydro[1,3]dioxolo[4,5-g]naphthalene}

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