(<(trifluoromethyl-3 phenyl)-4 piperazinyl-1>4 butyryl)-6 methyl-3 benzoxazolinone

Base Information

Chemical Name:(<(trifluoromethyl-3 phenyl)-4 piperazinyl-1>4 butyryl)-6 methyl-3 benzoxazolinone
CAS No.:124673-94-5
Molecular Formula:C₂₃H₂₄F₃N₃O₃
Molecular Weight:447.457
Hs Code.:

Synonyms:(<(trifluoromethyl-3 phenyl)-4 piperazinyl-1>4 butyryl)-6 methyl-3 benzoxazolinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (<(trifluoromethyl-3 phenyl)-4 piperazinyl-1>4 butyryl)-6 methyl-3 benzoxazolinone

Chemical Property:

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Technology Process of (<(trifluoromethyl-3 phenyl)-4 piperazinyl-1>4 butyryl)-6 methyl-3 benzoxazolinone

There total 3 articles about (<(trifluoromethyl-3 phenyl)-4 piperazinyl-1>4 butyryl)-6 methyl-3 benzoxazolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 124673-91-2
6-(4-bromobutyryl)-3-methyl-2,3-dihydro-2-oxo<1,3>benzoxazole

: 15532-75-9
1-(3-Trifluoromethylphenyl)piperazine

: 124673-94-5
(<(trifluoromethyl-3 phenyl)-4 piperazinyl-1>4 butyryl)-6 methyl-3 benzoxazolinone

Guidance literature:: With triethylamine; In benzene; for 15h; Heating;

Reference yield:

: 21892-80-8
3-methylbenzo[d]oxazol-2(3H)-one

: 124673-94-5
(<(trifluoromethyl-3 phenyl)-4 piperazinyl-1>4 butyryl)-6 methyl-3 benzoxazolinone

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / polyphosphoric acid / 0.75 h / 165 °C

2: 97 percent / HBr / acetone / 1 h / Ambient temperature

3: 89 percent / triethylamine / benzene / 15 h / Heating

With PPA; hydrogen bromide; triethylamine; In acetone; benzene;

Reference yield:

: 124673-90-1
6-(4-Hydroxy-butyryl)-3-methyl-3H-benzooxazol-2-one

: 124673-94-5
(<(trifluoromethyl-3 phenyl)-4 piperazinyl-1>4 butyryl)-6 methyl-3 benzoxazolinone

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / HBr / acetone / 1 h / Ambient temperature

2: 89 percent / triethylamine / benzene / 15 h / Heating

With hydrogen bromide; triethylamine; In acetone; benzene;