benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

Base Information

Chemical Name:benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester
CAS No.:894094-75-8
Molecular Formula:C₃₀H₃₃N₃O₇S
Molecular Weight:579.674
Hs Code.:

benzenesulfonic acid 4-[2-<i>tert</i>-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

Synonyms:benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

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Chemical Property of benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

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Technology Process of benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

There total 6 articles about benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: benzenesulfonic acid 4-[2-imino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester; compound with trifluoro-acetic acid

: 24424-99-5
di-tert-butyl dicarbonate

: 894094-75-8
benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; at 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2006.03.024

Reference yield:

: 894094-68-9
2-(4-benzenesulfonyloxy)benzyl-3-(4-methoxy-phenyl)-2-methylaminopropionic acid methyl ester

: 894094-75-8
benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / Et₃N; HgCl₂ / dimethylformamide / 12 h / 20 °C

2: 98 percent / 0.25 h / 20 °C

3: 82 percent / aq. NaHCO₃ / dioxane / 12 h / 20 °C

With sodium hydrogencarbonate; triethylamine; mercury dichloride; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2006.03.024

Reference yield:

: 894094-67-8
2-(4-benzenesulfonyloxy-benzyl)-2-(tert-butoxycarbonyl-methylamino)-3-(4-methoxy-phenyl)-propionic acid methyl ester

: 894094-75-8
benzenesulfonic acid 4-[2-tert-butoxycarbonylimino-4-(4-methoxy-benzyl)-3-methyl-5-oxo-imidazolidin-4-ylmethyl]-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / TFA / CH₂Cl₂ / 0 - 20 °C

2: 75 percent / Et₃N; HgCl₂ / dimethylformamide / 12 h / 20 °C

3: 98 percent / 0.25 h / 20 °C

4: 82 percent / aq. NaHCO₃ / dioxane / 12 h / 20 °C

With sodium hydrogencarbonate; triethylamine; trifluoroacetic acid; mercury dichloride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2006.03.024