[8-imino-7-(4-nitrophenyl)-7H,8H-12-oxa-9,11-diaza-benzo[a]anthracen-9-yl]-pyridyn-4-yl methylene amine

Base Information

Chemical Name:[8-imino-7-(4-nitrophenyl)-7H,8H-12-oxa-9,11-diaza-benzo[a]anthracen-9-yl]-pyridyn-4-yl methylene amine
CAS No.:606977-00-8
Molecular Formula:C₂₇H₁₈N₆O₃
Molecular Weight:474.478
Hs Code.:

Synonyms:[8-imino-7-(4-nitrophenyl)-7H,8H-12-oxa-9,11-diaza-benzo[a]anthracen-9-yl]-pyridyn-4-yl methylene amine

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Chemical Property of [8-imino-7-(4-nitrophenyl)-7H,8H-12-oxa-9,11-diaza-benzo[a]anthracen-9-yl]-pyridyn-4-yl methylene amine

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Technology Process of [8-imino-7-(4-nitrophenyl)-7H,8H-12-oxa-9,11-diaza-benzo[a]anthracen-9-yl]-pyridyn-4-yl methylene amine

There total 5 articles about [8-imino-7-(4-nitrophenyl)-7H,8H-12-oxa-9,11-diaza-benzo[a]anthracen-9-yl]-pyridyn-4-yl methylene amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 872-85-5
pyridine-4-carbaldehyde

: 606976-95-8
8-imino-7-(4-nitrophenyl)-7H,8H-12-oxa-9,11-diaza-benzo[a]anthracen-9-ylamine

: 606977-00-8
[8-imino-7-(4-nitrophenyl)-7H,8H-12-oxa-9,11-diaza-benzo[a]anthracen-9-yl]-pyridyn-4-yl methylene amine

Guidance literature:: With piperidine; In 1,4-dioxane; for 8h; Heating;

Reference yield:

: 90-15-3
α-naphthol

: 606977-00-8
[8-imino-7-(4-nitrophenyl)-7H,8H-12-oxa-9,11-diaza-benzo[a]anthracen-9-yl]-pyridyn-4-yl methylene amine

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / piperidine / ethanol / 3 h / Heating

2: 87 percent / acetic anhydride / 6 h / Heating

3: 90 percent / hydrazine hydrate / ethanol / 4 h

4: 65 percent / piperidine / dioxane / 8 h / Heating

With piperidine; hydrazine hydrate; In 1,4-dioxane; ethanol; acetic anhydride;

Reference yield:

: 2700-23-4
4-Nitrobenzylidenemalononitrile

: 606977-00-8
[8-imino-7-(4-nitrophenyl)-7H,8H-12-oxa-9,11-diaza-benzo[a]anthracen-9-yl]-pyridyn-4-yl methylene amine

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / piperidine / ethanol / 3 h / Heating

2: 87 percent / acetic anhydride / 6 h / Heating

3: 90 percent / hydrazine hydrate / ethanol / 4 h

4: 65 percent / piperidine / dioxane / 8 h / Heating

With piperidine; hydrazine hydrate; In 1,4-dioxane; ethanol; acetic anhydride;