3-methoxy-1-oxy>iodo>propyne

Base Information

Chemical Name:3-methoxy-1-oxy>iodo>propyne
CAS No.:134938-42-4
Molecular Formula:CF₃O₃S*C₁₀H₁₀IO
Molecular Weight:422.164
Hs Code.:

3-methoxy-1-<phenyl<<(trifluoromethyl)sulfonyl>oxy>iodo>propyne

Synonyms:3-methoxy-1-oxy>iodo>propyne

Suppliers and Price of 3-methoxy-1-oxy>iodo>propyne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methoxy-1-oxy>iodo>propyne

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-methoxy-1-oxy>iodo>propyne

There total 3 articles about 3-methoxy-1-oxy>iodo>propyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 129540-75-6
oxy>iodo>benzene

: 113794-24-4
tributyl-(3-methoxy-propyn-1-yl)stannane

: 134938-42-4
3-methoxy-1-oxy>iodo>propyne

Guidance literature:: In dichloromethane; at -40 ℃;
DOI:10.1021/ja00015a055

Reference yield: 76.0%

: 54339-94-5
1-bromo-3-methoxypropyne

: Trifluoro-methanesulfonatephenyl-((E)-2-trifluoromethanesulfonyloxy-vinyl)-iodonium;

: 134938-42-4
3-methoxy-1-oxy>iodo>propyne

Guidance literature:: 1-bromo-3-methoxypropyne; With n-butyllithium; In diethyl ether; hexane; toluene; at -78 ℃; for 0.25h;

Trifluoro-methanesulfonatephenyl-((E)-2-trifluoromethanesulfonyloxy-vinyl)-iodonium;; In diethyl ether; hexane; toluene; at -78 - 20 ℃;
DOI:10.1055/s-2000-6234

Reference yield:

: fluoro[trifluoromethanesulfonyloxy-λ³-iodanil]benzene

: 134938-42-4
3-methoxy-1-oxy>iodo>propyne

Guidance literature:: Multi-step reaction with 2 steps

1.1: CH₂Cl₂ / -78 °C

2.1: BuLi / toluene; diethyl ether; hexane / 0.25 h / -78 °C

2.2: 76 percent / toluene; diethyl ether; hexane / -78 - 20 °C

With n-butyllithium; In diethyl ether; hexane; dichloromethane; toluene; 1.1: Addition / 2.1: Metallation / 2.2: Substitution;
DOI:10.1055/s-2000-6234