2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-cyano-benzimidoyl chloride

Base Information

Chemical Name:2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-cyano-benzimidoyl chloride
CAS No.:1365992-03-5
Molecular Formula:C₁₃H₄Cl₄FN₃
Molecular Weight:363.005
Hs Code.:

Synonyms:2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-cyano-benzimidoyl chloride

Suppliers and Price of 2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-cyano-benzimidoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-cyano-benzimidoyl chloride

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-cyano-benzimidoyl chloride

There total 5 articles about 2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-cyano-benzimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1365992-02-4
2,6-dichloro-N-(2-chloro-3-fluoropyridin-4-yl)-4-cyano-benzamide

: 1365992-03-5
2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-cyano-benzimidoyl chloride

Guidance literature:: With thionyl chloride; for 18h; Reflux;

Reference yield:

: 628691-93-0
2-chloro-3-fluoro-pyridine-4-carboxylic acid

: 1365992-03-5
2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-cyano-benzimidoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: diphenyl phosphoryl azide / toluene / 3 h / 110 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

2.2: NH₂ cartridge

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h

3.2: 18 h

4.1: thionyl chloride / 18 h / Reflux

With thionyl chloride; diphenyl phosphoryl azide; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; toluene; mineral oil;

Reference yield:

: 1258298-06-4
2,6-dichloro-4-cyanobenzoyl chloride

: 1365992-03-5
2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-cyano-benzimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h

1.2: 18 h

2.1: thionyl chloride / 18 h / Reflux

With thionyl chloride; sodium hydride; In tetrahydrofuran; mineral oil;