1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole bis

Base Information

Chemical Name:1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole bis
CAS No.:95038-24-7
Molecular Formula:C₂₇H₃₃N₃O₄
Molecular Weight:463.577
Hs Code.:

1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole bis<N-(2-propyl)carbamate>

Synonyms:1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole bis

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Chemical Property of 1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole bis

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Technology Process of 1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole bis

There total 3 articles about 1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 103776-13-2
1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole

: 1795-48-8
Isopropyl isocyanate

: 95038-24-7
1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole bis

Guidance literature:: With dibutyltin diacetate; In dichloromethane; for 18h; Heating;
DOI:10.1021/jm00161a042

Reference yield:

: 3651-14-7
diethyl 3,5-diphenyl-1H-pyrrole-2,4-dicarboxylate

: 95038-24-7
1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole bis

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / K₂CO₃ / dimethylformamide / 48 h / 75 °C

2: 83 percent / LiAlH₄ / CH₂Cl₂; diethyl ether / 0.67 h / Heating

3: 65 percent / dibutyltin acetate / CH₂Cl₂ / 18 h / Heating

With lithium aluminium tetrahydride; dibutyltin diacetate; potassium carbonate; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00161a042

Reference yield:

: 103776-12-1
diethyl 3,5-diphenyl-1-methylpyrrole-2,4-dicarboxylate

: 95038-24-7
1-methyl-3,5-diphenyl-2,4-bis(hydroxymethyl)pyrrole bis

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / LiAlH₄ / CH₂Cl₂; diethyl ether / 0.67 h / Heating

2: 65 percent / dibutyltin acetate / CH₂Cl₂ / 18 h / Heating

With lithium aluminium tetrahydride; dibutyltin diacetate; In diethyl ether; dichloromethane;
DOI:10.1021/jm00161a042