ethyl 2-[6-(3-(ethoxymethoxy)naphthalen-2-yl)methoxy-3-oxo-3H-xanthen-9-yl]benzoate

Base Information

Chemical Name:ethyl 2-[6-(3-(ethoxymethoxy)naphthalen-2-yl)methoxy-3-oxo-3H-xanthen-9-yl]benzoate
CAS No.:1621132-83-9
Molecular Formula:C₃₆H₃₀O₇
Molecular Weight:574.63
Hs Code.:

Synonyms:ethyl 2-[6-(3-(ethoxymethoxy)naphthalen-2-yl)methoxy-3-oxo-3H-xanthen-9-yl]benzoate

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Chemical Property of ethyl 2-[6-(3-(ethoxymethoxy)naphthalen-2-yl)methoxy-3-oxo-3H-xanthen-9-yl]benzoate

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Technology Process of ethyl 2-[6-(3-(ethoxymethoxy)naphthalen-2-yl)methoxy-3-oxo-3H-xanthen-9-yl]benzoate

There total 5 articles about ethyl 2-[6-(3-(ethoxymethoxy)naphthalen-2-yl)methoxy-3-oxo-3H-xanthen-9-yl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1621132-82-8
2-(bromomethyl)-3-(ethoxymethoxy)naphthalene

: 72616-76-3
ethyl fluorescein

: 1621132-83-9
ethyl 2-[6-(3-(ethoxymethoxy)naphthalen-2-yl)methoxy-3-oxo-3H-xanthen-9-yl]benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1021/jo501116g

Reference yield:

: 2321-07-5,126605-73-0
fluorescein

: 1621132-83-9
ethyl 2-[6-(3-(ethoxymethoxy)naphthalen-2-yl)methoxy-3-oxo-3H-xanthen-9-yl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / ethanol / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

With boron trifluoride diethyl etherate; potassium carbonate; In ethanol; N,N-dimethyl-formamide; 2: |Williamson Ether Synthesis;
DOI:10.1021/jo501116g

Reference yield:

: 1621132-94-2
(3-(ethoxymethoxy)naphthalen-2-yl)methanol

: 1621132-83-9
ethyl 2-[6-(3-(ethoxymethoxy)naphthalen-2-yl)methoxy-3-oxo-3H-xanthen-9-yl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; triphenylphosphine; 1H-imidazole / dichloromethane / 0.5 h / 0 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

With 1H-imidazole; bromine; potassium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; 2: |Williamson Ether Synthesis;
DOI:10.1021/jo501116g