3-nitro-6-p-fluorobenzylaminopyridin-2-ylaminoformic acid tert-butyl ester

Base Information

Chemical Name:3-nitro-6-p-fluorobenzylaminopyridin-2-ylaminoformic acid tert-butyl ester
CAS No.:1609102-47-7
Molecular Formula:C₁₇H₁₉FN₄O₄
Molecular Weight:362.361
Hs Code.:

Synonyms:3-nitro-6-p-fluorobenzylaminopyridin-2-ylaminoformic acid tert-butyl ester

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Chemical Property of 3-nitro-6-p-fluorobenzylaminopyridin-2-ylaminoformic acid tert-butyl ester

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Technology Process of 3-nitro-6-p-fluorobenzylaminopyridin-2-ylaminoformic acid tert-butyl ester

There total 3 articles about 3-nitro-6-p-fluorobenzylaminopyridin-2-ylaminoformic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 33400-49-6
2-amino-3-nitro-6-(p-fluoro-benzylamino)-pyridine

: 1609102-47-7
3-nitro-6-p-fluorobenzylaminopyridin-2-ylaminoformic acid tert-butyl ester

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 40 ℃; Solvent; Temperature;

Reference yield:

: 27048-04-0
2-amino-6-chloro-3-nitropyridine

: 1609102-47-7
3-nitro-6-p-fluorobenzylaminopyridin-2-ylaminoformic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol / 10 h / 80 °C

2: sodium hydroxide / N,N-dimethyl-formamide / 40 °C

With triethylamine; sodium hydroxide; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 140-75-0
para-fluorobenzylamine

: 1609102-47-7
3-nitro-6-p-fluorobenzylaminopyridin-2-ylaminoformic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol / 10 h / 80 °C

2: sodium hydroxide / N,N-dimethyl-formamide / 40 °C

With triethylamine; sodium hydroxide; In methanol; N,N-dimethyl-formamide;